Design of spark plasma sintering parameters and preparation of Al2O3/TiB2/TiC micro–nano composite ceramic tool material. Issue 3 (2nd December 2022)

• Record Type: Journal Article
• Authors: Wang, Dong; Bai, Yifan; Qiu, Bo; Yu, Hongtao; Li, Zhibao
• Is Part Of: International journal of applied ceramic technology. Volume 20:Issue 3(2023)
• Page Start: 1420
• Page End: 1431
• Publication Date: 2022-12-02
• Subjects: cellular automata -- ceramic tool -- microstructure evolution simulation -- sintering parameters design -- spark plasma sintering; Ceramics -- Periodicals; Ceramics -- Technological innovations -- Periodicals; 620.1405
• DOI: 10.1111/ijac.14284
• Languages: English
• ISSNs: 1546-542X

Abstract

Abstract: A microstructure evolution model for the ceramic materials was constructed, and the spark plasma sintering parameters were optimized using the model to shorten the designing period and reduce the consumption of the material. Based on the optimized sintering parameters, the ceramic tool material with a composition of Al2 O3, TiB2, and TiC proved to be a success. It verified that the materials prepared under the optimized sintering parameters exhibited excellent mechanical properties. The results showed when sintered at 1600°C, under the pressure of 40 MPa and with the holding period of 7 min, the materials with 70% Al2 O3, 20% TiB2, and 10% nano‐TiC possess the relatively best performance, with the hardness, fracture toughness, and flexure strength being 20.3 GPa, 10.5 MPa/m 2, and 839.5 MPa, respectively.