A novel catalyst‐free mechanochemical protocol for the synthesis of 2, 3‐dihydro‐1H‐perimidines. (13th January 2020)
- Record Type:
- Journal Article
- Title:
- A novel catalyst‐free mechanochemical protocol for the synthesis of 2, 3‐dihydro‐1H‐perimidines. (13th January 2020)
- Main Title:
- A novel catalyst‐free mechanochemical protocol for the synthesis of 2, 3‐dihydro‐1H‐perimidines
- Authors:
- Harry, Nissy Ann
Radhika, Sankaran
Neetha, Mohan
Anilkumar, Gopinathan - Abstract:
- Abstract: A rapid, efficient, and green grinding assisted method for the synthesis of 2, 3‐dihydro‐1 H ‐perimidines has been developed. 1, 8‐Diaminonaphthalene and aldehydes were ground using mortar and pestle for 5 minutes affording the product in moderate to excellent yields. The methodology minimises the use of conventional workup and column chromatographic techniques. Abstract : Greener protocol for perimidine synthesis 25 examples Moderate to excellent yields Easy purification by recrystallization
- Is Part Of:
- Journal of heterocyclic chemistry. Volume 57:Number 4(2020)
- Journal:
- Journal of heterocyclic chemistry
- Issue:
- Volume 57:Number 4(2020)
- Issue Display:
- Volume 57, Issue 4 (2020)
- Year:
- 2020
- Volume:
- 57
- Issue:
- 4
- Issue Sort Value:
- 2020-0057-0004-0000
- Page Start:
- 2037
- Page End:
- 2043
- Publication Date:
- 2020-01-13
- Subjects:
- aldehyde -- grinding -- ketone -- mechanochemistry -- perimidine
Heterocyclic compounds -- Periodicals
547.59 - Journal URLs:
- http://onlinelibrary.wiley.com/ ↗
- DOI:
- 10.1002/jhet.3880 ↗
- Languages:
- English
- ISSNs:
- 0022-152X
- Deposit Type:
- Legaldeposit
- View Content:
- Available online (eLD content is only available in our Reading Rooms) ↗
- Physical Locations:
- British Library DSC - 4998.200000
British Library DSC - BLDSS-3PM
British Library STI - ELD Digital store - Ingest File:
- 26759.xml