A new high temperature, high heating rate, low axial gradient capillary heater. (18th November 2022)

• Record Type: Journal Article
• Authors: Marshall, Kenneth P.; Emerich, Hermann; McMonagle, Charles J.; Fuller, Chloe A.; Dyadkin, Vadim; Chernyshov, Dmitry; van Beek, Wouter
• Is Part Of: Journal of synchrotron radiation. Volume 30:Part 1(2023)
• Page Start: 267
• Page End: 272
• Publication Date: 2022-11-18
• Subjects: capillary heater -- X‐ray scattering -- X‐ray absorption; Synchrotron radiation -- Periodicals; Free electron lasers -- Periodicals; 539.73505
• DOI: 10.1107/S1600577522009845
• Languages: English
• ISSNs: 0909-0495

Abstract

Abstract : A new high‐temperature capillary heater design suitable for synchrotron X‐ray diffraction, total scattering and EXAFS experiments is described. Abstract : A new heater design, capable of fast heating and cooling to and from >1000°C, has been developed at the Swiss–Norwegian Beamlines, European Synchrotron Radiation Facility, France. The design uses a SiC head to distribute heat, and resistive Si3 N4 heat cartridges to provide heat.