Beamline-implemented stretching devices for in situ X-ray scattering experiments. Issue 1 (1st December 2022)

• Record Type: Journal Article
• Authors: Euchler, E; Sambale, A K; Schneider, K; Uhlig, K; Boldt, R; Stommel, M; Stribeck, A; Schwartzkopf, M; Rothkirch, A; Roth, S V
• Is Part Of: Journal of physics. Volume 2380 Issue 1(2022)
• Publication Date: 2022-12-01
• Subjects: Physics -- Congresses; 530.5
• DOI: 10.1088/1742-6596/2380/1/012109
• Languages: English
• ISSNs: 1742-6588

Abstract

Abstract: Two recently developed experimental devices for investigating soft matter deformation are presented. Both devices exploit the capabilities of a modern synchrotron beamline to enable advanced and highly precise materials-science experiments in which X-ray scattering is registered. The devices can be operated both in monotonic as well as cyclic mode and are implemented into a beamline at DESY, Hamburg (Germany). Hence, relevant experimental parameters, such as displacement, force and temperature, are recorded synchronously with the individual X-ray scattering patterns. In addition, spatial variation of materials deformation can be monitored and recorded with optical microscopy. This unique sample environment enables in situ X-ray experiments in transmission, i.e. small- or wide-angle X-ray scattering (SAXS or WAXS), and in grazing-incidence geometry, i.e. grazing-incidence (GI-) SAXS or WAXS. One device with stepper motors is designed for studies of slow, (quasi-) static deformation and the other one with pneumatic actuators can be used for fast, impact deformation. Both devices are available to external beamline users, too.