Characterization of micro-sandwich structures via direct ink writing epoxy based cores. (January 2023)

• Record Type: Journal Article
• Authors: Smith, Zane J; Barsoum, Demiana R; Arwood, Zachariah L; Penumadu, Dayakar; Advincula, Rigoberto C
• Other Names: Krueger Ronald guest-editor.; Ratcliffe James G guest-editor.
• Is Part Of: Journal of sandwich structures & materials. Volume 25:Number 1(2023)
• Page Start: 112
• Page End: 127
• Publication Date: 2023-01
• Subjects: additive manufacturing -- direct ink writing -- epoxy resin -- hybrid manufacturing -- sandwich structures; Sandwich construction -- Periodicals; 624.177905
• DOI: 10.1177/10996362221118329
• Languages: English
• ISSNs: 1099-6362

Abstract

Sandwich structured (SS) composites demonstrate considerable flexural stiffness and high strength-to-weight ratios and can be tailored as functional materials. Historically they have been constrained to specific material types and geometry due to limitations in manufacturing methods. However, employing additive manufacturing (AM), specifically direct ink writing (DIW), can provide an alternative method for making SS composites with complex and controllable micro and mesostructures with multifunctionality targeted at desired mechanical, thermal, and electrical properties. DIW, an extrusion-based AM technique, uses a viscous and thixotropic ink with desired components that, once printed, is cured to obtain the final complex net shape parts. In this paper, a novel hybrid AM technique is employed to manufacture SS composite materials containing bisphenol A-based epoxy core and carbon fiber reinforced polymer (CFRP) face sheets that are fabricated via DIW and vacuum infusion process (VIP), respectfully. We demonstrate that the fabrication of these SS composites can be tailored from a thermosetting material, from which additives and/or various lattice structures can be manufactured to achieve enhanced and desirable mechanical integrity with functional properties. Surface topology and mechanical testing techniques are used to characterize the fabricated hybrid SS composites to study and assess mechanical stability. A rheo-kinetic cure model was developed for the core material to allow for additive manufacturing process requirements while ensuring complete cross-linking for the thermoset-based core material. Because of the ability to obtain relatively small core-thickness and controlled architecture, this method now allows for fabricating layered micro-sandwich structures for realizing further light-weighting in relevant applications.