Synthesis of new 3-phenyl Substituted Dibenzo-1, 4-diazepin-1-one Derivatives. (November 2014)

• Record Type: Journal Article
• Authors: Wang, Fang-Ming; Bao, Dan; Wang, Ming; Li, Ming-Jun; Chen, Li-Zhuang; Han, Guang-Fan
• Is Part Of: Journal of chemical research. Volume 38:Number 11(2014)
• Page Start: 664
• Page End: 667
• Publication Date: 2014-11
• Subjects: 3-phenyldibenzo-1, 4-diazepin-1-one -- 5-phenylcyclohexane-1, 3-dione -- condensation -- crystal structure; Chemistry -- Research -- Periodicals; Chemistry -- Periodicals; 540.5
• DOI: 10.3184/174751914X14138073011066
• Languages: English
• ISSNs: 1747-5198

Abstract

A new series of 3-phenyl substituted dibenzo-1, 4-diazepin-1-one derivatives were synthesised by condensation of 5-phenylcyclohexane-1, 3-dione, o -phenylenediamine and benzaldehydes. All the compounds were characterised by IR, MS, 1 H NMR and elemental analysis. The crystal structure of 3-phenyl-11-(2-chlorophenyl)-2, 3, 4, 5, 10, 11-hexahydro-1H-dibenzo[b, e] [1, 4]diazepin-1-one was determined by X-ray single-crystal diffraction.