Investigation of the in situ thermal conductivity and absorption behavior of nanocomposite powder materials in laser powder bed fusion processes. (March 2021)

• Record Type: Journal Article
• Authors: Pannitz, O.; Lüddecke, A.; Kwade, A.; Sehrt, J.T.
• Is Part Of: Materials & design. Volume 201(2021)
• Publication Date: 2021-03
• Subjects: Additive manufacturing -- PBF-LB/M -- Stainless steel (1.4404 -- 316 L) -- Nanocomposite -- Absorption -- Infrared thermography; Materials -- Periodicals; Engineering design -- Periodicals; Matériaux -- Périodiques; Conception technique -- Périodiques; Electronic journals; 620.11
• DOI: 10.1016/j.matdes.2021.109530
• Languages: English
• ISSNs: 0264-1275

Abstract

Abstract: One of the AM processes for direct manufacturing of metallic components is powder bed fusion of metals using a laser beam system (PBF-LB/M), in which metallic powders are molten and solidified in a layer upon layer manner by a focused laser beam. In recent years, the focus has initially been on increasing the efficiency of the systems itself. However, the modification of standard AM metal alloys using nanoparticles offers the possibility to improve the PBF-LB/M-process concerning its process efficiency and actual densification and thermal conductivity. In this work, a methodology for an in-situ investigation of the thermal conductivity as well as the reflectance behavior of metallic powder materials during the PBF-LB/M-process is established. The powder material stainless steel 1.4404 was coated with different nanoparticles (few-layer graphene (FLG), silicon carbide (SiC)) and processed in a standardized build process. As a result, the reflectance rate of all modified materials could be increased. Besides, the thermal conductivity of the material is attested to be a decisive and influencing factor for the quality of the final component. Thus, an improved relative density was achieved using the FLG/1.4404 and SiC/1.4404 (1 vol%) due to the increased thermal conductivity of the material. Also significant defects in the cross section were visible at SiC/1.4404 (4 vol%). Graphical abstract: Unlabelled Image Highlights: Stainless steel powder 1.4404 is successfully coated with silicon carbide (SiC) and few-layer graphene (FLG). The developed SiC and FLG coated 1.4404 powder exhibits a decreased reflectance. SiC (1 vol%) and FLG (0.75 vol%) coatings improve the relative density of upskin specimens to 99.9%. The addition of SiC (4 vol%) leads to a decrease in relative density of approx. 93.9%. The FLG coating leads to a rapid heat dissipation into the already solidified underlying layers during the melting process.