Effect of helium as process gas on laser powder bed fusion of Ti-6Al-4V studied with operando diffraction and radiography. Issue 1 (31st December 2022)

• Record Type: Journal Article
• Authors: Pauzon, Camille; Van Petegem, Steven; Hryha, Eduard; Sin Ting Chang, Cynthia; Hocine, Samy; Van Swygenhoven, Helena; de Formanoir, Charlotte; Dubiez-Le Goff, Sophie
• Is Part Of: European Journal of Materials. Volume 2:Issue 1(2022)
• Page Start: 422
• Page End: 435
• Publication Date: 2022-12-31
• Subjects: Helium -- laser powder bed fusion -- operando radiography -- operando X-ray diffraction -- process gas -- spatters; 620.11
• DOI: 10.1080/26889277.2022.2081622
• Languages: English
• ISSNs: 2688-9277

Abstract

Abstract: The utilisation of helium as process gas in laser powder bed fusion limits the generation of Ti-6Al-4V hot and incandescent spatters and enhances their cooling rate. In the present study, operando X-ray diffraction using synchrotron X-rays permits to verify that the cooling rates experienced by the deposited material are not significantly affected by the process gas unlike spatters. Topography measurements of the top printed surface reveal lower roughness of He-produced samples, attributed to the previously observed reduction of spatters with He and thus a reduction of redepositions on the powder bed and printed surfaces. Operando radiography provides with insights on the spatter formation mechanisms namely particle entrainment, agglomeration, melting and spheroidization. Highlights: The top surface average roughness of samples produced with He is lower than that of Ar equivalent Deposited Ti-6Al-4V cooling rates during LPBF are not significantly affected by the use of He Grain size and orientation of Ti-6Al-4V is similar when processing under Ar, He, and a mixture of both Operando radiography permits to identify the mechanisms of Ti-6Al-4V spatter formation