One-step synthesis of lead zirconate titanate particles using a solid-state reaction method. Issue 3 (March 2022)

• Record Type: Journal Article
• Authors: Hidayat, Darmawan; Taufik, Mohammad; Setianto, Setianto
• Is Part Of: Heliyon. Volume 8:Issue 3(2022)
• Publication Date: 2022-03
• Subjects: Ceramic material -- Piezoelectric -- Perovskite -- Shaker milling -- Solid-state reaction; Research -- Periodicals; Medical sciences -- Periodicals; Natural history -- Periodicals; Social sciences -- Periodicals; Earth sciences -- Periodicals; Physical sciences -- Periodicals; 507.2
• DOI: 10.1016/j.heliyon.2022.e09125
• Languages: English
• ISSNs: 2405-8440

Abstract

Abstract: This study aims to determine the one-step synthesis of lead zirconate titanate (PbZr(1-x) Tix O3 ; PZT) particles, using a solid-state reaction method. These particles were synthesized at x of 0.48, using a solid-state reaction (SSR) method at various operating temperatures of 700–1000 °C. Before the reaction in a muffle furnace, the precursor powder was shaker milled for 2 h. The structural analysis of the diffraction patterns showed the formation of the PZT perovskite particles. It also showed the evolution from the tetragonal phase (at 800 and 900 °C) to the coexistence of tetragonal and rhombohedral stages in samples synthesized at 1000 °C. Furthermore, the crystallite particle size synthesized and commercialized at 1000 °C were 36.00 and 47.98 nm, respectively. These showed the formation of monodispersed size distribution, with an average of approximately 4.7 μm. Therefore, the PZT particles were successfully synthesized through a one-step synthesis, using the SSR method with a pre-mixed shaker milling. Abstract : Ceramic material; Piezoelectric; Perovskite; Shaker milling; Solid-state reaction.