Efficient and stereoselective synthesis of thiosulfinates from disulfide using cumene hydroperoxide in the presence of titanium-based catalyst systems. Issue 9 (3rd May 2019)
- Record Type:
- Journal Article
- Title:
- Efficient and stereoselective synthesis of thiosulfinates from disulfide using cumene hydroperoxide in the presence of titanium-based catalyst systems. Issue 9 (3rd May 2019)
- Main Title:
- Efficient and stereoselective synthesis of thiosulfinates from disulfide using cumene hydroperoxide in the presence of titanium-based catalyst systems
- Authors:
- Sun, Pengju
Huang, Jiansheng
Xu, Jinyi
Yu, Niefang - Abstract:
- Abstract: An efficient and stereoselective procedure of oxidizing disulfide to thiosulfinate 2a using CHP as the oxidant and economically available Ti(O-i-Pr)4 /L-DET/H2 O as catalysts were developed. The reaction went smoothly under mild conditions with synthetic useful yield and the workup for obtaining the final product is quite convenient. GRAPHICAL ABSTRACT:
- Is Part Of:
- Synthetic communications. Volume 49:Issue 9(2019)
- Journal:
- Synthetic communications
- Issue:
- Volume 49:Issue 9(2019)
- Issue Display:
- Volume 49, Issue 9 (2019)
- Year:
- 2019
- Volume:
- 49
- Issue:
- 9
- Issue Sort Value:
- 2019-0049-0009-0000
- Page Start:
- 1165
- Page End:
- 1172
- Publication Date:
- 2019-05-03
- Subjects:
- FK228 -- HDAC -- oxidation -- stereoselective -- thiosulfinates
Organic compounds -- Synthesis -- Periodicals
Chemistry, Organic
Synthesis
547.205 - Journal URLs:
- http://www.tandfonline.com/toc/lsyc20/current ↗
http://www.tandfonline.com/ ↗ - DOI:
- 10.1080/00397911.2019.1590847 ↗
- Languages:
- English
- ISSNs:
- 0039-7911
- Deposit Type:
- Legaldeposit
- View Content:
- Available online (eLD content is only available in our Reading Rooms) ↗
- Physical Locations:
- British Library DSC - 8586.830000
British Library DSC - BLDSS-3PM
British Library STI - ELD Digital store - Ingest File:
- 20399.xml