Microstructure control and mechanical properties of directionally solidified large size TiAl alloy by electromagnetic confinement. (January 2022)

• Record Type: Journal Article
• Authors: Yue, Xiao'an; Shen, Jun; Xiong, Yilong; Zheng, Shaokai
• Is Part Of: Intermetallics. Volume 140(2022)
• Publication Date: 2022-01
• Subjects: Titanium aluminides -- Nanoindentation hardness -- Room-temperature tensile property -- Full lamellae -- Seed; Intermetallic compounds -- Metallography -- Periodicals; Metallic glasses -- Periodicals; Composés intermétalliques -- Métallographie -- Périodiques; 669.94
• DOI: 10.1016/j.intermet.2021.107406
• Languages: English
• ISSNs: 0966-9795

Abstract

Abstract: Ti–48Al–2Nb–2Cr alloys with a diameter of 30 mm were prepared by electromagnetic confinement directional solidification with Ti–43Al–3Si seed under different pulling rates. The macro/microstructure evolution and mechanical properties of the directionally solidified Ti–48Al–2Nb–2Cr alloys were investigated. With increasing pulling rates, the grain sizes of the directionally solidified alloys increase to the maximum at the pulling rate of 15 μm/s and then decrease. During the process of directional solidification, the primary phase of the alloy transforms from the α phase into β phase with the increase of pulling rates. At the pulling rate of 5 μm/s, the equiaxed grains with fully lamellar microstructure are formed, and some B2 phases and massive γ phases are found at the grain boundary. The well aligned α2 /γ lamellar orientation is obtained at the pulling rate of 15 μm/s, while the inclined lamellar orientation is obtained when the pulling rate increases to 20 μm/s. The interlamellar spacing (λ) decreases with increasing pulling rate ( V ) according to the relationship λ = 6966 V − 0.563 and r 2 = 0.986 . For the DS samples, the nanoindentation hardness of the lamellae and the interlamellar spacing satisfy the relationship of H N = 53.83 d − 0.309 and r 2 2 = 0.96 . The room-temperature tensile strength of directionally solidified alloy reaches the maximum value at the pulling rate of 15 μm/s. The fracture changes from interlamellar to translamellar mode with increasing pulling rate. The synergistic effect of nanotwins and dislocations contributes to the relatively high room-temperature tensile strength and elongation during the deformation. Highlights: The directionally solidified TiAl alloy exhibits excellent mechanical property at room temperature and high temperature. However, the size of the TiAl alloy prepared by traditional directional solidification method is too small. In this work, Ti–48Al–2Nb–2Cr alloy with a diameter of 30 mm was prepared by EMCDS with Ti–43Al–3Si seed. The effect of pulling rates on the macrostructure, primary phase, lamellar spacing, lamellar orientation is studied. The mechanical properties on nanoindentation hardness and room temperature tensile property are investigated.