A convenient synthesis and crystal structure of disubstituted 1, 2, 3-triazoles having ether functionality. Issue 24 (17th December 2019)

• Record Type: Journal Article
• Authors: Luxmi, Raj; Kaushik, C. P.; Kumar, Devinder; Kumar, Krishan; Pahwa, Ashima; Sangwan, Jyoti; Chahal, Manisha
• Is Part Of: Synthetic communications. Volume 49:Issue 24(2019)
• Page Start: 3435
• Page End: 3441
• Publication Date: 2019-12-17
• Subjects: Disubstituted 1, 2, 3-triazoles -- synthesis -- X-ray crystallography; Organic compounds -- Synthesis -- Periodicals; Chemistry, Organic; Synthesis; 547.205
• DOI: 10.1080/00397911.2019.1672744
• Languages: English
• ISSNs: 0039-7911

Abstract

Abstract: A series of 27 ether-linked 1, 4-disubstituted 1, 2, 3-triazoles (8a–8z1 ) has been synthesized by 1, 3 dipolar cycloaddition of 1-substituted-4-(prop-2-yn-1-yloxy)benzene (3a–3c ) and aromatic azides (5a–5c, 7a–7f ). The synthesized compounds were explicated by FTIR, 1 H NMR, 13 C NMR and HRMS techniques. The structures of synthesized triazoles 8c (CCDC 1840219) and 8f (CCDC 1840220) were also confirmed by X-ray crystallography. GRAPHICAL ABSTRACT: