Polymer film dewetting for fabrication of out-of-autoclave prepreg with high through-thickness permeability. (November 2018)

• Record Type: Journal Article
• Authors: Schechter, Sarah G.K.; Centea, Timotei; Nutt, Steven R.
• Is Part Of: Composites. Volume 114(2018)
• Page Start: 86
• Page End: 96
• Publication Date: 2018-11
• Subjects: A. Prepreg -- A. Polymer-matrix composites -- B. Porosity -- E. Out of autoclave processing; Composite materials -- Periodicals; Manufacturing processes -- Periodicals; Composite materials; Manufacturing processes; Periodicals; 620.11805
• DOI: 10.1016/j.compositesa.2018.08.002
• Languages: English
• ISSNs: 1359-835X

Abstract

Abstract: Polymer film dewetting on a substrate (independent of fiber bed architecture) was explored, developed, and demonstrated as a method to produce out-of-autoclave, vacuum bag-only (OoA/VBO) prepregs with high transverse permeability and process robustness. The dimensions of the surface openings created by dewetting were measured, and the percent surface area exposed was calculated. Prepregs were fabricated with continuous and dewetted (discontinuous) films to produce trial laminates. The laminates were cured under both standard and sub-optimal conditions, and were characterized before, during, and after cure. Laminates fabricated with dewetted resin consistently achieved near-zero porosity. In contrast, laminates with continuous film displayed high levels of porosity, particularly during sub-optimal cure. The findings demonstrate that dewetting can be used effectively to produce OoA prepregs with high through-thickness permeability, which can yield porosity-free laminates via VBO processing. Furthermore, these results elucidate aspects of resin dewetting that are critical in the creation of robust OoA prepregs.