X-ray refraction distinguishes unprocessed powder from empty pores in selective laser melting Ti-6Al-4V. Issue 2 (1st February 2018)

• Record Type: Journal Article
• Authors: Laquai, R.; Müller, B. R.; Kasperovich, G.; Haubrich, J.; Requena, G.; Bruno, G.
• Is Part Of: Materials research letters. Volume 6:Issue 2(2018)
• Page Start: 130
• Page End: 135
• Publication Date: 2018-02-01
• Subjects: Additive manufacturing -- X-ray refraction -- microscopy -- porosity -- X-ray-computed tomography; Materials science -- Research -- Periodicals; Biomedical materials -- Research -- Periodicals; Composite materials -- Research -- Periodicals; Biomedical materials -- Research; Composite materials -- Research; Materials science -- Research; Periodicals; 620.1105
• DOI: 10.1080/21663831.2017.1409288
• Languages: English
• ISSNs: 2166-3831

Abstract

ABSTRACT: For the first time, X-ray refraction techniques are proven for the identification of void formation in Ti-6Al-4V parts produced by selective laser melting. The topology and volume fraction of pores are measured in samples produced with different laser energy density. Unique X-ray refraction methods identify different kinds of defects, characteristic to the regions below and above the optimum laser energy density, namely unprocessed powder (unmolten powder particles, balling effect, and fusion defects) from empty keyhole pores. Furthermore, it is possible to detect small inhomogeneities (voids or cracks) with sizes below the spatial resolution of optical microscopy and X-ray computed tomography. IMPACT STATEMENT For the first time, we show that, unparalleled by high-resolution X-ray-computed tomography or electron microscopy, X-ray refraction can distinguish unprocessed powder from empty pores in additive manufactured materials. GRAPHICAL ABSTRACT: