Deformation of Mg-γMg17Al12in situ composites: Room temperature mechanical behaviour, microstructures and mechanisms. (May 2021)

• Record Type: Journal Article
• Authors: Donnadieu, Patricia; Benrhaiem, Souad; Renou, Gilles; Zhang, Chunyang; Tassin, Catherine; Blandin, Jean-Jacques
• Is Part Of: Intermetallics. Volume 132(2021)
• Publication Date: 2021-05
• Subjects: Intermetallics -- Complex metallic alloys -- Mg–Al alloys -- In situ composite -- Eutectic -- Room temperature deformation; Intermetallic compounds -- Metallography -- Periodicals; Metallic glasses -- Periodicals; Composés intermétalliques -- Métallographie -- Périodiques; 669.94
• DOI: 10.1016/j.intermet.2021.107127
• Languages: English
• ISSNs: 0966-9795

Abstract

Abstract: Deformation tests at room temperature have been carried out on a series of in situ Mg-γMg17 Al12 composites with volume fraction of γMg17 Al12 phase varying between 20% and 60%. Regardless of the phase volume fraction, these Mg-γMg17 Al12 composites that are prepared by solidification consist in magnesium-rich dendrites and a eutectic mixture. The eutectic mixture is made of magnesium fibres embedded in a matrix formed by the γMg17 Al12 phase, a hard and brittle complex metallic alloy. Compression tests at room temperature have shown that a global plastic deformation is observed even though the soft phase is always enclosed in the brittle one. According to the strain-stress curve, deformation proceeds in two stages: a first stage at low stress (σ ~ 100 MPa) and low strain (Δε < 0.01) almost similar for all the composites and a second stage characterized by a strain hardening effect along with a significant deformation for composites with γ phase volume fraction smaller than 40%, whereas no or little additional deformation is observed for composites with volume fraction higher than 40% that break at high stress (~400 MPa). Microstructural observations of the deformed samples have evidenced dislocations in the γMg17 Al12 matrix and their localization as pile-ups and slip bands as well as the transmission of deformation across the eutectic mixture. The plasticity of the γMg17 Al12 phase and the mechanical behaviour of the Mg-γMg17 Al12 composites are discussed with respect to the microstructure characteristics and to the specific atomic features of complex metallic alloy phases. Graphical abstract: Image 1 Highlights: In situ composites consisting in Mg dendrites and Mg-γMg17Al12 eutectic mixture. The soft Mg phase is always embedded in the hard and brittle γ-phase. However the Mg-γ composites exhibit a macroscopic deformation at room temperature. Evidence of dislocations crossing the Mg phase and the submicronic γ phase domains. a combination of size reduction, soft inclusion effect and complex alloy structure.