Multiresidue Analysis of Insecticides and Other Selected Environmental Contaminants in Poultry Manure by Gas Chromatography/Mass Spectrometry. (27th November 2019)

• Record Type: Journal Article
• Authors: Aznar, Ramón; Albero, Beatriz; Sánchez-Brunete, Consuelo; Miguel, Esther; Tadeo, José L
• Is Part Of: Journal of AOAC International. Volume 97:Number 4(2014)
• Page Start: 978
• Page End: 986
• Publication Date: 2019-11-27
• Subjects: Agricultural chemistry -- Periodicals; Food -- Analysis -- Periodicals; 543
• DOI: 10.5740/jaoacint.SGEAznar
• Languages: English
• ISSNs: 1060-3271

Abstract

Abstract: An analytical method was developed for the simultaneous determination in poultry manure of 41 organic contaminants belonging to different chemical classes: pesticides, polycyclic aromatic hydrocarbons, polychlorinated biphenyls, and polybrominated diphenyl ethers. Poultry manure was extracted with a modified QuEChERS method, and the extracts were analyzed by isotope dilution GC/MS. Recovery of these contaminants from samples spiked at levels ranging from 25 to 100 ng/g was satisfactory for all the compounds. The developed procedure provided LODs from 0.8 to 9.6 ng/g. The analysis of poultry manure samples collected on different farms confirmed the presence of some of the studied contaminants. Pyrethroids and polycyclic aromatic hydrocarbons were the main contaminants detected. DDT and its metabolite DDE were also found but at relatively low concentrations.