Continuous flow synthesis of 2, 2′-diselenobis(benzoic acid) and derivatives. Issue 4 (2nd March 2020)

• Record Type: Journal Article
• Authors: Begini, Francesca; Krasowska, Dorota; Jasiak, Aleksandra; Drabowicz, Jozef; Santi, Claudio; Sancineto, Luca
• Is Part Of: Reaction chemistry & engineering. Volume 5:Issue 4(2020)
• Page Start: 641
• Page End: 644
• Publication Date: 2020-03-02
• Subjects: Reaction mechanisms (Chemistry) -- Periodicals; Chemical engineering -- Periodicals; Chemical engineering; Reaction mechanisms (Chemistry); Periodicals; 547.705
• DOI: 10.1039/d0re00012d
• Languages: English
• ISSNs: 2058-9883

Abstract

Abstract : The continuous flow synthesis of the key building block 2, 2′-diselenobis(benzoic acid) (DSBA) and its analogues is herein reported. Abstract : The continuous flow synthesis of the key building block 2, 2′-diselenobis(benzoic acid) (DSBA) is herein reported. Water was used as a solvent in a reaction time as short as 90 s. This provided a successful strategy for the synthesis of DSBA which was obtained in excellent yield. The optimized procedure has been extended to DSBA derivatives.