Alumina–MWCNT composites: microstructural characterization and mechanical properties. Issue 1 (2nd January 2019)

• Record Type: Journal Article
• Authors: Sharma, Nidhi; Syed, Alam Nasimul; Ray, Bankim Chandra; Yadav, Surekha; Biswas, Krishanu
• Is Part Of: Journal of Asian ceramic societies. Volume 7:Issue 1(2019)
• Page Start: 1
• Page End: 19
• Publication Date: 2019-01-02
• Subjects: Alumina -- carbon nanotubes -- spark plasma sintering -- wear -- fracture toughness; Ceramics -- East Asia -- Periodicals; Materials science -- Periodicals; 620.1405
• DOI: 10.1080/21870764.2018.1552235
• Languages: English
• ISSNs: 2187-0764

Abstract

ABSTRACT: In the present work, Al2 O3 –multiwalled carbon nanotube (MWCNT) composites have been developed by both conventional sintering and spark plasma sintering (SPS) and their microstructures, mechanical properties and wear behavior have been investigated. Further, the influence of various other parameters such as the sintering time, sintering temperature, MWCNT loading level and processing technique adopted for development of the composites has also been analyzed. The powder metallurgy route was selected for development of Al2 O3 –0.2, 0.5, 0.8, 3, 5 vol% MWCNT composites using both conventional sintering and SPS. For conventionally sintered Al2 O3 –MWCNT composites, it has been found that both the hardness and relative density of the composites decreased up to a loading level of 0.2 vol% of MWCNTs, followed by a continuous increase with the addition of MWCNTs to the Al2 O3 matrix, attaining a maximum value in the case of Al2 O3 –3 vol% MWCNT composite. The wear behavior of conventionally sintered composites also exhibits significant improvement with increase in sintering time. The SPSed Al2 O3 –MWCNT composites show a much higher relative density and better mechanical and tribological properties as compared to conventionally sintered Al2 O3 –MWCNT composites.