Multi-frequency dynamic-mechanical thermal analysis of methyl methacrylate adhesive (MMA). Issue 2 (17th February 2019)

• Record Type: Journal Article
• Authors: Bula, Arkadiusz; Jurczyk, Sebastian; Chmielnicki, Błażej; Hulimka, Jacek; Kozłowski, Marcin
• Is Part Of: International journal of polymer analysis and characterization. Volume 24:Issue 2(2019)
• Page Start: 169
• Page End: 177
• Publication Date: 2019-02-17
• Subjects: Methacrylate adhesive -- DMTA -- master curve; Polymers -- Analysis -- Periodicals; 547.705
• DOI: 10.1080/1023666X.2018.1564126
• Languages: English
• ISSNs: 1023-666X

Abstract

Abstract: The paper presents the results of Dynamic-Mechanical Thermal Analysis (DMTA) for a selected methacrylate adhesive at the frequency range from 1 to 50 Hz and the heating rate of 1 and 3 °C/min, in the range from –70 °C to 180 °C. On the basis of the test results, the glass transition temperature was evaluated for three calculation methods. Master curves were also designated for three different reference temperatures: –20, +20 and +60 °C. Master curves were calculated using shift factors a T - calculated by numerical method.