A convenient synthesis of 4-amino-2-fluoro-N-methyl-benzamide. (1st October 2013)
- Record Type:
- Journal Article
- Title:
- A convenient synthesis of 4-amino-2-fluoro-N-methyl-benzamide. (1st October 2013)
- Main Title:
- A convenient synthesis of 4-amino-2-fluoro-N-methyl-benzamide
- Authors:
- Xu, Defeng
Xu, Xing
Zhu, Zhiling - Abstract:
- A convenient and concise synthesis of 2-Fluoro-4-nitrobenzoic acid was obtained by oxidation of 2-fluoro-4-nitrotoluene with potassium permanganate in the presence of a phase transfer catalyst in 74% yield. N-methyl-2-fluoro-4-nitrobenzamide was then produced via chlorination and amination in 95% yield. Hydrogenation in the presence of Pd/C can afforded 4-amino-2-fluoro-N-methyl-benzamide in 98% yield
- Is Part Of:
- Journal of chemical research. Volume 37:Number 10(2013)
- Journal:
- Journal of chemical research
- Issue:
- Volume 37:Number 10(2013)
- Issue Display:
- Volume 37, Issue 10 (2013)
- Year:
- 2013
- Volume:
- 37
- Issue:
- 10
- Issue Sort Value:
- 2013-0037-0010-0000
- Page Start:
- 615
- Page End:
- 616
- Publication Date:
- 2013-10-01
- Subjects:
- Chemistry -- Research -- Periodicals
Chemistry -- Periodicals
540.5 - Journal URLs:
- http://stl.publisher.ingentaconnect.com/content/stl/jcr ↗
https://journals.sagepub.com/home/chl ↗
http://www.sciencereviews2000.co.uk/ ↗ - DOI:
- 10.3184/174751913X13787959772340 ↗
- Languages:
- English
- ISSNs:
- 1747-5198
- Deposit Type:
- Legaldeposit
- View Content:
- Available online (eLD content is only available in our Reading Rooms) ↗
- Physical Locations:
- British Library DSC - BLDSS-3PM
British Library STI - ELD Digital store - Ingest File:
- 9610.xml