Microstructure and thermomechanical characteristics of spark plasma sintered TiC ceramics doped with nano-sized WC. Issue 2 (1st February 2019)

• Record Type: Journal Article
• Authors: Sabahi Namini, Abbas; Ahmadi, Zohre; Babapoor, Aziz; Shokouhimehr, Mohammadreza; Shahedi Asl, Mehdi
• Is Part Of: Ceramics international. Volume 45:Issue 2(2019)Part A
• Page Start: 2153
• Page End: 2160
• Publication Date: 2019-02-01
• Subjects: Titanium carbide -- Spark plasma sintering -- Tungsten carbide -- Microstructure -- Thermomechanical characteristics; Ceramics -- Periodicals; Céramique industrielle -- Périodiques; Ceramics; Periodicals; Electronic journals; 666
• DOI: 10.1016/j.ceramint.2018.10.125
• Languages: English
• ISSNs: 0272-8842

Abstract

Abstract: In this study, we studied the effects of nano-sized WC addition (0, 1.5 and 3 wt%) on microstructure and thermomechanical properties of TiC-based ceramics. WC-doped TiC matrix composites were sintered by spark plasma at 1900 °C under 40 MPa for 7 min. The densification behavior of WC-doped TiC ceramics was characterized and compared with the monolithic TiC. Microstructural investigation of the sintered specimens was achieved by scanning electron microscopy. X-ray diffraction analysis was carried out to determine the phase evolution of the prepared ceramics. In addition, the thermal and mechanical characteristics including thermal conductivity, Vickers hardness and flexural strength were evaluated and their relationship with the microstructural features was discussed. Thermal conductivity increment and the relevant pronounced effects on grain growth inhibition were observed for TiC-3 wt% WC. The obtained results demonstrated that the addition of 3 wt% WC plays a vital role in sinterability enhancement of TiC by accelerating the densification. The highest relative density (99.9%), Vickers hardness (28.6 GPa) and flexural strength (620 MPa) were obtained for the TiC ceramic doped with 3 wt% nano-sized WC.