Behaviour of pre-stressed T91 and ODS steels exposed to liquid lead-bismuth eutectic. (February 2018)

• Record Type: Journal Article
• Authors: Hojna, Anna; Hadraba, Hynek; Di Gabriele, Fosca; Husak, Roman
• Is Part Of: Corrosion science. Volume 131(2018)
• Page Start: 264
• Page End: 277
• Publication Date: 2018-02
• Subjects: Steel -- SEM -- Oxidation -- Liquid metal embrittlement; Corrosion and anti-corrosives -- Periodicals; 620.11223
• DOI: 10.1016/j.corsci.2017.12.005
• Languages: English
• ISSNs: 0010-938X

Abstract

Graphical abstract: Highlights: Bend specimens were exposed to liquid lead-bismuth at 350° C up to 2000 h. Thin protective oxide layers; continuous on T91 and discontinuous on the ODS steels. T91: the inner oxidation zone was wavy under tension and straight without stress. No tendency to oxide failure, no LME crack. Abstract: Structural materials compatibility in conditions relevant to plant operation is of primary importance to safety. The work describes the behaviour of T91 and ferritic ODS steels, 14%Cr and 19%Cr under such conditions. Three-point-bend specimens were pre-stressed up to yield strength, then exposed to flowing lead-bismuth eutectic in a loop at 350° C for 500 and 1000 h, in non-flowing one for 2000 h. The oxygen content was measured to be in the order of 10 −5 wt.%. Post-test examination by means of microhardness and SEM with EDS demonstrated the formation of thin oxides without crack initiation, which is discussed. Because it was not observed either direct contact between the steels and LBE or local high plastic deformation, no LME occurred.