Warming up for mechanosynthesis – temperature development in ball mills during synthesis. Issue 10 (18th January 2017)

• Record Type: Journal Article
• Authors: Kulla, Hannes; Wilke, Manuel; Fischer, Franziska; Röllig, Mathias; Maierhofer, Christiane; Emmerling, Franziska
• Is Part Of: Chemical communications. Volume 53:Issue 10(2017)
• Page Start: 1664
• Page End: 1667
• Publication Date: 2017-01-18
• Subjects: Chemistry -- Periodicals; 540
• DOI: 10.1039/c6cc08950j
• Languages: English
• ISSNs: 1359-7345

Abstract

Abstract : We present a first direct measurement of the temperature during milling combined with in situ Raman spectroscopy monitoring. Abstract : We present a first direct measurement of the temperature during milling combined with in situ Raman spectroscopy monitoring. The data reveal a low temperature increase due to the mechanical impact and clear temperature increases as a consequence of the reaction heat. Based on the data, temperature rises as postulated in the magma plasma and hot spot theory can be excluded for soft matter milling syntheses.