Efficient Preparation of Alkaloids Polycarpine and Polycarpaurines A and C. (30th October 2015)
- Record Type:
- Journal Article
- Title:
- Efficient Preparation of Alkaloids Polycarpine and Polycarpaurines A and C. (30th October 2015)
- Main Title:
- Efficient Preparation of Alkaloids Polycarpine and Polycarpaurines A and C
- Authors:
- Guo, Pengbin
Yan, Shuang
Hu, Zeliang
Zhuang, Weihui
Xiong, Yan
Zhang, Lanya
Wang, Ziwen
Wang, Qingmin - Abstract:
- Abstract : An efficient method for the preparation of alkaloids polycarpine and polycarpaurines A and C via microwave‐assisted three‐stepone‐pot reaction as the key step has been developed. This is the first report about the synthesis of polycarpaurines A and C. Starting from commercially available p ‐methoxybenzaldehyde, polycarpine and polycarpaurine A were obtained over seven steps with 40 and 24 % overall yield, respectively. Polycarpine could convert to polycarpaurine C in 72% yield in the presence of NaHSO3 . The structure of polycarpine and polycarpaurines A and C was confirmed by 1 H NMR, 13 C NMR, and HRMS. Abstract :
- Is Part Of:
- Journal of heterocyclic chemistry. Volume 54:Number 1(2017:Jan.)
- Journal:
- Journal of heterocyclic chemistry
- Issue:
- Volume 54:Number 1(2017:Jan.)
- Issue Display:
- Volume 54, Issue 1 (2017)
- Year:
- 2017
- Volume:
- 54
- Issue:
- 1
- Issue Sort Value:
- 2017-0054-0001-0000
- Page Start:
- 121
- Page End:
- 124
- Publication Date:
- 2015-10-30
- Subjects:
- Heterocyclic compounds -- Periodicals
547.59 - Journal URLs:
- http://onlinelibrary.wiley.com/ ↗
- DOI:
- 10.1002/jhet.2549 ↗
- Languages:
- English
- ISSNs:
- 0022-152X
- Deposit Type:
- Legaldeposit
- View Content:
- Available online (eLD content is only available in our Reading Rooms) ↗
- Physical Locations:
- British Library DSC - 4998.200000
British Library DSC - BLDSS-3PM
British Library STI - ELD Digital store - Ingest File:
- 2532.xml