Diamond beamline I07: a beamline for surface and interface diffraction. (27th July 2016)

• Record Type: Journal Article
• Authors: Nicklin, Chris; Arnold, Tom; Rawle, Jonathan; Warne, Adam
• Is Part Of: Journal of synchrotron radiation. Volume 23:Part 5(2016)
• Page Start: 1245
• Page End: 1253
• Publication Date: 2016-07-27
• Subjects: X‐ray diffraction -- surface -- structure -- reflectivity -- grazing incidence -- surface structure -- interfaces -- X‐ray scattering; Synchrotron radiation -- Periodicals; Free electron lasers -- Periodicals; 539.73505
• DOI: 10.1107/S1600577516009875
• Languages: English
• ISSNs: 0909-0495

Abstract

Abstract : A beamline is described for grazing‐incidence X‐ray diffraction at Diamond Light Source that houses two experimental hutches, the first housing a large multi‐circle diffractometer on which a wide variety of sample environments can be mounted and the second with an ultrahigh‐vacuum system on the diffractometer to enable in situ studies of molecular beam epitaxy. Techniques available include X‐ray reflectivity, surface X‐ray diffraction, grazing‐incidence small‐angle X‐ray scattering, grazing‐incidence wide‐angle X‐ray scattering and grazing‐incidence diffraction. Abstract : Beamline I07 at Diamond Light Source is dedicated to the study of the structure of surfaces and interfaces for a wide range of sample types, from soft matter to ultrahigh vacuum. The beamline operates in the energy range 8–30 keV and has two endstations. The first houses a 2+3 diffractometer, which acts as a versatile platform for grazing‐incidence techniques including surface X‐ray diffraction, grazing‐incidence small‐ (and wide‐) angle X‐ray scattering, X‐ray reflectivity and grazing‐incidence X‐ray diffraction. A method for deflecting the X‐rays (a double‐crystal deflector) has been designed and incorporated into this endstation, extending the surfaces that can be studied to include structures formed on liquid surfaces or at liquid–liquid interfaces. The second experimental hutch contains a similar diffractometer with a large environmental chamber mounted on it, dedicated to in situ ultrahigh‐vacuum studies. It houses a range of complementary surface science equipment including a scanning tunnelling microscope, low‐energy electron diffraction and X‐ray photoelectron spectroscopy ensuring that correlations between the different techniques can be performed on the same sample, in the same chamber. This endstation allows accurate determination of well ordered structures, measurement of growth behaviour during molecular beam epitaxy and has also been used to measure coherent X‐ray diffraction from nanoparticles during alloying.