Microwave assisted synthesis of a mono organoimido functionalized Anderson polyoxometalate. Issue 48 (19th November 2015)

• Record Type: Journal Article
• Authors: Ritchie, C.; Bryant, G.
• Is Part Of: Dalton transactions. Volume 44:Issue 48(2015)
• Page Start: 20826
• Page End: 20829
• Publication Date: 2015-11-19
• Subjects: Chemistry, Inorganic -- Periodicals; Chemistry, Physical and theoretical -- Periodicals; Chemistry, Inorganic -- Periodicals; 546.05
• DOI: 10.1039/c5dt04000k
• Languages: English
• ISSNs: 1477-9226

Abstract

Abstract : The synthesis of an aliphatic organoimido functionalized polyoxometalate has been achieved through a microwave assisted reaction protocol in the absence of any activating reagents. Abstract : The synthesis of an aliphatic organoimido functionalized polyoxometalate has been achieved through a microwave assisted reaction protocol in the absence of any activating reagents. Characterization of the pendant amine containing polyanion [Mo6 O18 NC(OCH2 )3 MnMo6 O18 (OCH2 )3 CNH2 ] 5− (1) includes single crystal XRD, NMR, ESI-MS, IR and SAXS.