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Diversity-oriented synthesis of fused thioglycosyl benzo[e][1, 4]oxathiepin-5-ones and benzo[f][1, 4]thiazepin-5(2H)-ones by a sequence of palladium-catalyzed glycosyl thiol arylation and deprotection–lactonization reactions. Issue 44 (15th September 2015)
Record Type:
Journal Article
Title:
Diversity-oriented synthesis of fused thioglycosyl benzo[e][1, 4]oxathiepin-5-ones and benzo[f][1, 4]thiazepin-5(2H)-ones by a sequence of palladium-catalyzed glycosyl thiol arylation and deprotection–lactonization reactions. Issue 44 (15th September 2015)
Main Title:
Diversity-oriented synthesis of fused thioglycosyl benzo[e][1, 4]oxathiepin-5-ones and benzo[f][1, 4]thiazepin-5(2H)-ones by a sequence of palladium-catalyzed glycosyl thiol arylation and deprotection–lactonization reactions
Abstract : An efficient synthesis of thioglycosylated benzo[ e ][1, 4]-oxathiepin-5-one and benzothiazepinone derivatives has been reported. Abstract : An efficient synthesis of thioglycosylated benzo[ e ][1, 4]oxathiepin-5-one and benzothiazepinone derivatives by a sequence of palladium-catalyzed glycosyl thiol arylation followed by deprotection–lactonization reactions has been reported. This diversity-oriented strategy enabled access to unknown complex cyclic scaffolds with polyhydroxylated appendages of biological interest.