Fatigue stipulation of bulk-fill composites: An in vitro appraisal. Issue 9 (September 2015)

• Record Type: Journal Article
• Authors: Vidhawan, Shruti A.; Yap, Adrian U.; Ornaghi, Barbara P.; Banas, Agnieszka; Banas, Krzysztof; Neo, Jennifer C.; Pfeifer, Carmem S.; Rosa, Vinicius
• Is Part Of: Dental materials. Volume 31:Issue 9(2015)
• Page Start: 1068
• Page End: 1074
• Publication Date: 2015-09
• Subjects: Dentistry -- Periodicals; Dental materials -- Periodicals; 617.695
• DOI: 10.1016/j.dental.2015.06.006
• Languages: English
• ISSNs: 0109-5641

Abstract

<abstract abstract-type="author" id="abs0005"> <title id="sect0005">Abstract</title> <sec> <title id="sect0010">Objectives</title> <p id="spar0005">The aim of this study was to determine the Weibull and slow crack growth (SCG) parameters of bulk-fill resin based composites. The strength degradation over time of the materials was also assessed by strength-probability-time (SPT) analysis.</p> </sec> <sec> <title id="sect0015">Methods</title> <p id="spar0010">Three bulk-fill [Tetric EvoCeram Bulk Fill (TBF); X-tra fil (XTR); Filtek Bulk-fill flowable (BFL)] and a conventional one [Filtek Z250 (Z250)] were studied. Seventy five disk-shaped specimens (12 mm in diameter and 1 mm thick) were prepared by inserting the uncured composites in a stainless steel split mold followed by photoactivation (1200 mW/cm<sup>2</sup>/20 s) and storage in distilled water (37 °C/24 h). Degree of conversion was evaluated in five specimens by analysis of FT-IR spectra obtained in the mid-IR region. The SCG parameters <italic>n</italic> (stress corrosion susceptibility coefficient) and <italic>σ</italic><sub>f0</sub> (scaling parameter) were obtained by testing ten specimens in each of the five stress rates: 10<sup>−2</sup>, 10<sup>−1</sup>, 10<sup>0</sup>, 10<sup>1</sup> and 10<sup>2</sup> MPa/s using a piston-on-three-balls device. Weibull parameter <italic>m</italic> (Weibull modulus) and <italic>σ</italic><sub>f0</sub> (characteristic strength) were obtained by testing additional 20 specimens at 1 MPa/s. Strength–probability–time (SPT) diagrams were constructed by merging SCG and Weibull parameters.</p> </sec> <sec> <title id="sect0020">Results</title> <p id="spar0015">BFL and TBF presented higher <italic>n</italic> values, respectively (40.1 and 25.5). Z250 showed the highest (157.02 MPa) and TBF the lowest (110.90 MPa) <italic>σ</italic><sub>f0</sub> value. Weibull analysis showed <italic>m</italic> (Weibull modulus) of 9.7, 8.6, 9.7 and 8.9 for TBF, BFL, XTR and Z250, respectively. SPT diagram for 5% probability of failure showed strength decrease of 18% for BFL, 25% for TBF, 32% for XTR and 36% for Z250, respectively, after 5 years as compared to 1 year.</p> </sec> <sec> <title id="sect0025">Significance</title> <p id="spar0020">The reliability and decadence of strength over time for bulk-fill resin composites studied are, at least, comparable to conventional composites. BFL shows the highest fatigue resistance under all simulations followed by TBF, while XTR was at par with Z250.</p> </sec> </abstract>