<abstract abstract-type="main" xml:lang="en"> <title>Abstract</title> <p>A composite of the electronic conductor α‐LiFeO<sub>2</sub> and the insulator γ‐LiAlO<sub>2</sub> is prepared by solid state reaction of a 1:0.7:0.3 molar mixture of Li<sub>2</sub>CO<sub>3</sub>, Fe<sub>2</sub>O<sub>3</sub>, and Al<sub>2</sub>O<sub>3</sub> (900 °C, 1 h).</p> </abstract>