Handbook of heavy oil properties and analysis. (2023)

• Record Type: Book
• Further Information: Note: James G. Speight.
• Authors: Speight, James G
• Contents: Preface Chapter 1: History and Terminology 1.0 Introduction 2.0 Historical Perspectives 2.1 Pre-Christian Era Use of Heavy Oil and Bitumen 2.2 Post-Christian Era Use of Heavy Oil and Bitumen 3.0 Definitions and Terminology 3.1 Non-Viscous Feedstocks 3.1.1 Crude Oil 3.1.2 Opportunity Crude Oil 3.1.3 High Acid Crude Oil 3.1.4 Foamy Oil 3.2 Viscous Feedstocks 3.2.1 Gas Oil 3.2.2 Heavy Crude Oil 3.2.3 Extra Heavy Crude Oil 3.2.4 Tar Sand Bitumen 3.2.5 Residua 3.2.6 Asphalt 3.2.7 Tar and Pitch 3.2.8 Sludge 4.0 Classification 5.0 Feedstock Evaluation 6.0 Modern Analytical Perspectives 7.0 References Chapter 2: Sampling and Measurement 1.0 Introduction 2.0 Sampling 2.1 Sampling Protocol 2.1.1 Sampling Semi-Volatile and Non-Volatile Compounds 2.1.2 Solids 2.1.3 Extract Concentration 2.1.4 Sample Cleanup 2.2 Representative Sample 2.3 Sampling Error 3.0 Measurement 4.0 Method Validation 4.1 Requirements 4.2 Method Detection Limit 4.3 Accuracy 4.4 Precision 5.0 Quality Control and Quality Assurance 5.1 Quality Control 5.2 Quality Assurance 6.0 Assay and Specifications 6.1 Assay 6.2 Specifications 6.3 Metallic Constituents 6.4 Water Content 7.0 Environmental Issues 8.0 References Chapter 3: Chemical Composition 1.0 Introduction 2.0 Elemental Composition 3.0 Chemical Composition 3.1 Hydrocarbon Constituents 3.1.1 Paraffin Hydrocarbon Derivatives 3.1.2 Cycloparaffin Hydrocarbon Derivatives 3.1.3 Aromatic Hydrocarbon Derivatives 3.1.4 Unsaturated Hydrocarbon Derivatives 3.2 Non-hydrocarbon Constituents 3.2.1 Sulfur Compounds 3.2.2 Nitrogen Compounds 3.2.3 Oxygen Compounds 3.3 Metallic Constituents 3.4 Porphyrins 4.0 Chemical Composition by Distillation 4.1 Vacuum Gas Oil 4.2 Vacuum Residua 5.0 Composition by Spectroscopic Methods 5.1 Infrared Spectroscopy 5.2 Nuclear Magnetic Resonance Spectroscopy 5.3 Mass Spectrometry 5.4 Other Techniques 6.0 References Chapter 4: Fractional Composition 1.0 Introduction 2.0 Distillation 3.0 Solvent Treatment 3.1 Asphaltene Separation 3.1.1. Influence of Solvent Type 3.1.2 Influence of the Degree of Dilution 3.1.3 Influence of Temperature 3.1.4. Influence of Contact Time 3.2 Fractionation 4.0 Adsorption Methods 4.1 Chemical Factors 4.2 Fractionation Methods 5.0 Chemical Methods 6.0 The Asphaltene Fraction 7.0 Carbenes and Carboids 8.0 References Chapter 5: Chemical Properties 1.0 Introduction 2.0 Acid Number 3.0 Elemental Analysis and Metals 4.0 Emulsion Formation 5.0 Evaporation 6.0 Flash Point and Fire Point 7.0 Functional Group Analysis 8.0 Halogenation 9.0 Hydrogenation 10.0 Oxidation 11.0 Thermal Methods 12.0 Miscellaneous Methods 13.0 References Chapter 6: Physical Properties, Electrical Properties, and Optical Properties 1.0 Introduction 2.0 Physical Properties 2.1 Adhesion 2.2 Density and Specific Gravity 2.3 Surface and Interfacial Tension 2.4 Viscosity 3.0 Electrical Properties 3.1 Conductivity 3.2 Dielectric Constant 3.3 Dielectric Strength 3.4 Dielectric Loss and Power Factor 3.5 Static Electrification 4.0 Optical Properties 4.1 Optical Activity 4.2 Refractive Index 5.0 References Chapter 7: Thermal Properties 1.0 Introduction 2.0 Ash Production 3.0 Carbon Residue 4.0 Critical Properties 5.0 Enthalpy 6.0 Heat of Combustion 7.0 Latent Heat 8.0 Liquefaction and Solidification 9.0 Pour Point 10.0 Pressure-Volume-Temperature Relationships 11.0 Softening Point 12.0 Specific Heat 13.0 Thermal Conductivity 14.0 Volatility 15.0 References Chapter 8: Chromatographic Analysis 1.0 Introduction 2.0 Adsorption Chromatography 3.0 Gas Chromatography 4.0 Gel Permeation Chromatography 5.0 High-Performance Liquid Chromatography 6.0 Ion-Exchange Chromatography 7.0 Simulated Distillation 8.0 Supercritical Fluid Chromatography 9.0 Thin Layer Chromatography 10.0 References Chapter 9: Structural Group Analysis 1.0 Introduction 2.0 Physical Property Methods 2.3 Density Method 2.6 Density-Temperature Coefficient Method 2.1 Direct Method 2.5 Dispersion-Refraction Method 2.2 Waterman Ring Analysis 2.7 Molecular Weight-Refractive Index Method 2.4 N-D-M Method 2.8 Miscellaneous Methods 3.0 Spectroscopic Methods 3.1 Electron Spin Resonance 3.2 Infrared Spectroscopy 3.3 Mass Spectrometry 3.4 Nuclear Magnetic Resonance Spectroscopy 3.5 Ultraviolet Spectroscopy 3.6 X-ray Diffraction 4.0 H
• Edition: 1st
• Publisher Details: Hoboken : John Wiley & Sons, Inc
• Publication Date: 2023
• Extent: 1 online resource (496 pages)
• Subjects: 553.282; Heavy oil -- Analysis; Heavy oil -- Testing; Analytical chemistry
• Languages: English
• ISBNs: 9781119577102
• Related ISBNs: 9781119577157
• Notes: Note: Includes bibliographical references and index.; Note: Description based on CIP data; resource not viewed.
• Access Rights: Legal Deposit; Only available on premises controlled by the deposit library and to one user at any one time; The Legal Deposit Libraries (Non-Print Works) Regulations (UK).
• Access Usage: Restricted: Printing from this resource is governed by The Legal Deposit Libraries (Non-Print Works) Regulations (UK) and UK copyright law currently in force.