The systematic identification of organic compounds. (2023)
- Record Type:
- Book
- Title:
- The systematic identification of organic compounds. (2023)
- Main Title:
- The systematic identification of organic compounds.
- Authors:
- Hermann, Christine K. F
Morrill, Terence C
Shriner, Ralph Lloyd, 1899-1994
Fuson, Reynold C (Reynold Clayton), 1895-1979 - Other Names:
- Shriner, Ralph Lloyd, 1899-1994
- Contents:
- Preface Chapter 1 Introduction 1.1 The Systematic Identification of Organic Compounds: 1.2 Suggestions to Students and Instructors Chapter 2 Laboratory Safety 2.1 Working Safely in the Laboratory 2.2 Training 2.3 Personal Protection Equipment 2.4 Safety Data Sheets 2.5 Storage of Chemicals 2.6 Disposal of Chemicals 2.7 Safely Using Equipment in the Laboratory Chapter 3 Identification of Unknowns 3.1 Discussion of Report Form 3.2 Preliminary Examination 3.3 Physical Properties 3.4 Molecular Weight Determination 3.5 Molecular Formula Determination 3.6 Solubility Tests 3.7 Infrared, Nuclear Magnetic Resonance, and Mass Spectra Analyses 3.8 Classification Tests 3.9 Preparation of a Satisfactory Derivative 3.10 Mixtures 3.11 Report Forms Chapter 4 Preliminary Examination, Physical Properties, and Elemental Analysis 4.1 Preliminary Examination 4.2 Determination of Physical Properties 4.3 Optical Rotation 4.4 Recrystallization 4.5 Qualitative Elemental Analysis 4.6 Quantitative Elemental Analysis Chapter 5 Classification of Organic Compounds by Solubility 5.1 Solubility in Water, Aqueous Acids and Bases, and Ether 5.2 Solubility in Organic Solvents Chapter 6 Separation of Mixtures 6.1 Preliminary Examination of Mixtures 6.2 Distillation and Sublimation 6.3 Extractions: Separation Based Upon Salt Formation 6.4 Chromatography Chapter 7 Nuclear Magnetic Resonance Spectrometry 7.1 Theory of Nuclear Magnetic Resonance 7.2 Preparation of the Sample 7.3 Proton Spectra 7.4 Carbon-13Preface Chapter 1 Introduction 1.1 The Systematic Identification of Organic Compounds: 1.2 Suggestions to Students and Instructors Chapter 2 Laboratory Safety 2.1 Working Safely in the Laboratory 2.2 Training 2.3 Personal Protection Equipment 2.4 Safety Data Sheets 2.5 Storage of Chemicals 2.6 Disposal of Chemicals 2.7 Safely Using Equipment in the Laboratory Chapter 3 Identification of Unknowns 3.1 Discussion of Report Form 3.2 Preliminary Examination 3.3 Physical Properties 3.4 Molecular Weight Determination 3.5 Molecular Formula Determination 3.6 Solubility Tests 3.7 Infrared, Nuclear Magnetic Resonance, and Mass Spectra Analyses 3.8 Classification Tests 3.9 Preparation of a Satisfactory Derivative 3.10 Mixtures 3.11 Report Forms Chapter 4 Preliminary Examination, Physical Properties, and Elemental Analysis 4.1 Preliminary Examination 4.2 Determination of Physical Properties 4.3 Optical Rotation 4.4 Recrystallization 4.5 Qualitative Elemental Analysis 4.6 Quantitative Elemental Analysis Chapter 5 Classification of Organic Compounds by Solubility 5.1 Solubility in Water, Aqueous Acids and Bases, and Ether 5.2 Solubility in Organic Solvents Chapter 6 Separation of Mixtures 6.1 Preliminary Examination of Mixtures 6.2 Distillation and Sublimation 6.3 Extractions: Separation Based Upon Salt Formation 6.4 Chromatography Chapter 7 Nuclear Magnetic Resonance Spectrometry 7.1 Theory of Nuclear Magnetic Resonance 7.2 Preparation of the Sample 7.3 Proton Spectra 7.4 Carbon-13 Spectra 7.5 DEPT 7.6 COSY 7.7 HSQC Chapter 8 Infrared Spectrometry 8.1 Theory of Infrared Spectrometry 8.2 Preparation of the Sample 8.3 Functional Group Identification Chapter 9 Mass Spectrometry 9.1 Theory of Mass Spectrometry 9.2 Cleavage Reactions Chapter 10 Chemical Tests for Functional Groups 10.1 Acid Anhydrides 10.2 Acyl Halides 10.3 Alcohols 10.4 Aldehydes 10.5 Amides 10.6 Amines and Amine Salts 10.7 Amino Acids 10.8 Carbohydrates 10.9 Carboxylic Acids 10.10 Esters 10.11 Ethers 10.12 Halides 10.13 Hydrocarbons -- Alkanes 10.14 Hydrocarbons -- Alkenes 10.15 Hydrocarbons -- Alkynes 10.16 Hydrocarbons -- Aromatic 10.17 Ketones 10.18 Nitriles 10.19 Nitro Compounds 10.20 Phenols 10.21 Sulfonamides, Sulfonic Acids, and Sulfonyl Chlorides Chapter 11 The Preparation of Derivatives 11.1 Carboxylic Acids, Acid Anhydrides, and Acid Halides 11.2 Alcohols 11.3 Aldehydes and Ketones 11.4 Amides 11.5 Amines 11.6 Amino Acids 11.7 Carbohydrates 11.8 Esters 11.9 Ethers -- Aliphatic 11.10 Ethers -- Aromatic 11.11 Halides -- Alkyl 11.12 Halides -- Aromatic 11.13 Hydrocarbons -- Aromatic 11.14 Nitriles 11.15 Nitro Compounds 11.16 Phenols 11.17 Sulfonic Acids, Sulfonyl Chlorides, and Sulfonamides Chapter 12 Structural Problems 12.1 Compounds with Structures Previously Described in the Literature 12.2 Determination of the Structure of New Compounds Not Described in the Chemical Literature 12.3 Problems Chapter 13 Chemical Literature 13.1 Handbooks 13.2 Compendia 13.3 Spectral Collections 13.4 Journals 13.5 Abstracts and Indexes 13.6 Monographs Appendix I Handy Tables for the Organic Lab Appendix II Tables of Derivatives Appendix III Equipment and Chemicals for the Laboratory Index … (more)
- Edition:
- Ninth edition
- Publisher Details:
- Hoboken : John Wiley & Sons, Inc
- Publication Date:
- 2023
- Extent:
- 1 online resource (704 pages)
- Subjects:
- 547.0078
Chemistry, Organic -- Laboratory manuals - Languages:
- English
- ISBNs:
- 9781119799689
- Related ISBNs:
- 9781119799665
- Notes:
- Note: Includes bibliographical references and index.
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- Physical Locations:
- British Library HMNTS - ELD.DS.769598
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