50 and more essential NMR experiments : a detailed guide /: a detailed guide. (2014)

• Record Type: Book
• Other Titles: Fifty and more essential NMR experiments
• Further Information: Note: Matthias Findeisen, Stefan Berger.
• Other Names: Findeisen, Matthias; Berger, Stefan
• Contents: Cover; Title Page; Preface; Contents; Chapter 1 The Organic Set of NMR Spectra; 1.1 The 1H NMR Experiment; 1.2 APT-13C NMR; 1.3 COSY; 1.4 NOESY; 1.5 HSQC; 1.6 HMBC; Chapter 2 Advanced Organic NMR Spectroscopy; 2.1 2D J-Resolved 1H NMR Spectroscopy; 2.2 ROESY; 2.3 TOCSY; 2.4 HSQC-TOCSY; 2.5 HOESY; 2.6 INADEQUATE; 2.7 ADEQUATE; 2.8 J-HMBC; 2.9 Gated Decoupling; Chapter 3 Selective Methods; 3.1 Water suppression by Presaturation; 3.2 Solvent Suppression by 1D-NOESY; 3.3 Water Suppression by SOGGY Excitation Sculpting; 3.4 Solvent Suppression using WET; 3.5 SELTOCSY; 3.6 SELNOESY; 3.7 SELINCOR. 3.8 SELINQUATE3.9 Band Selective HMBC; Chapter 4 Heteronuclear NMR; 4.1 11B NMR Spectroscopy; 4.2 15N NMR Spectroscopy; 4.3 17O NMR Spectroscopy; 4.4 19F NMR Spectroscopy; 4.5 29Si NMR Spectroscopy; 4.6 57Fe NMR Spectroscopy; 4.7 195Pt NMR Spectroscopy; Chapter 5 Experiments in Physical Organic Chemistry; 5.1 Measurement of the Spin-Lattice Relaxation Time T1; 5.2 Measurement of the Spin-Spin Relaxation Time T2; 5.3 Dynamic 1H NMR Spectroscopy; 5.4 Diffusion Measurement with DOSY; 5.5 Residual Dipolar Couplings (RDC); Chapter 6 Organic Chemistry Applications; 6.1 ASIS. 6.2 Chirality Determination6.3 Advanced Mosher Method; 6.4 Quantitative NMR and Relaxation Reagents; 6.5 Determination of Association Constants Ka; 6.6 STD NMR; 6.7 A Kinetic Experiment; Chapter 7 An Excursion to the Solid State and to Structural Biology; 7.1 The CP/MAS Experiment; 7.2 High-Resolution Magic-Angle Spinning; 7.3 HN-HSQC; 7.4 HNCA; Chapter 8 Maintenance and Calibration; 8.1 Calibration of Pulse Duration in the Transmitter Channel; 8.2 Calibration of the Pulse Duration in the Indirect Channel; 8.3 Shaped Pulses; 8.4 Adiabatic pulses; 8.5 Temperature Calibration in NMR. 8.6 Calibration of Pulsed Field GradientsAppendix; Answers; Pulse Programs; Elementary Product Operator Formalism Rules; Chemical Shift and Spin-Coupling Data for Strychnine; Picture Credits; Index.
• Publisher Details: Weinheim : Wiley-VCH Verlag GmbH & Co. KGaA
• Publication Date: 2014
• Extent: 1 online resource (308 pages), illustrations (some color)
• Subjects: 543.66; Nuclear magnetic resonance spectroscopy; SCIENCE -- Chemistry -- Analytic; Nuclear magnetic resonance spectroscopy; Electronic books
• Languages: English
• ISBNs: 9783527336968; 3527336966; 1299804209; 9781299804203; 3527334831; 9783527334834; 9783527336944; 9783527336975; 3527336974
• Related ISBNs: 352733694X; 9783527334834
• Notes: Note: Includes bibliographical references and index.
• Access Rights: Legal Deposit; Only available on premises controlled by the deposit library and to one user at any one time; The Legal Deposit Libraries (Non-Print Works) Regulations (UK).
• Access Usage: Restricted: Printing from this resource is governed by The Legal Deposit Libraries (Non-Print Works) Regulations (UK) and UK copyright law currently in force.