Traceability, validation and measurement uncertainty in chemistry. Practical examples / Vol. 3, ([2019])

• Record Type: Book
• Further Information: Note: Nineta Hrastelj, Ricardo Bettencourt da Silva.
• Editors: Hrastelj, Nineta; Silva, Ricardo Bettencourt da
• Contents: Intro; Foreword; Preface; Contents; Editors and Contributors; 1 Measurement of Total Reactive Phosphorus in Natural Water by Molecular Spectrophotometry (SMEWW 4500-P D); 1 Brief Description of the Analytical Procedure; 1.1 Introduction; 1.2 Determination of Reactive Phosphorus in Natural Water by Molecular Spectrophotometry; 2 The Customer's Requirements Concerning Quality of the Measurement Result; 3 Validation of the Measurement Procedure -- Relevant Equations and Measurement Data; 4 Measurement Uncertainty of the Result: Relevant Equations and Measurement Data; 4.1 Equations 4.2 Experimental Data of Sample AnalysisExercise 1: Establishing Traceability in Analytical Chemistry; Exercise 2: The Customer's Requirements Concerning Quality of the Measurement Result; Exercise 3: Enlarge the Analytical Method Scope; Exercise 4: Building an Uncertainty Budget; References; 2 Measurement of Concentration of Nitrate in Drinking Water; 1 Description of the Analytical Procedure; 1.1 Scope; 1.1.1 General; 1.1.2 Interferences; 1.2 Principle; 1.3 Reagents; 1.3.1 Eluents; 1.3.2 Water; 1.3.3 CRM -- Nitrate in Water; 1.4 Apparatus; 1.5 Quality Requirements of the Separating Column 1.6 Sampling and Samples1.7 Procedure; 1.8 Calculation; 2 The Customer's Requirements Concerning Quality of the Measurement Result; 3 Validation of the Measurement Procedure -- Relevant Equations and Measurement Data; 4 Measurement Uncertainty of the Result -- Relevant Equations and Measurement Data; Exercise 1: Establishing Traceability in Analytical Chemistry; Exercise 2: Single Laboratory Validation of Measurement Procedures; Part I: General Issues; Part II: Parameters to be Validated; Part III: Some Calculations and Conclusions; Exercise 3: Building an Uncertainty Budget; Sec24 3 Measurement of Moisture Content (Water Content) in Edible Oil Using the Volumetric Karl Fischer Method According to ISO 8534:19961 Description of the Analytical Procedure; 1.1 Principle; 1.2 Scope; 1.3 Procedure; 1.4 Interferences; 1.5 Equipment and Reagents; 1.6 Sampling and Sample Pre-treatment; 1.7 Calculation; 1.8 Results; 2 The Customer's Requirement Concerning Quality of the Measurement Result; 3 Validation Data of the Measurement Procedure -- Relevant Equations and Measurement Data; 3.1 Equations; 3.2 Validation Data 4 Measurement Uncertainty of the Result -- Relevant Equations and Measurement Data4.1 Equations for Uncertainty Calculation by the ISO GUM Modelling (Bottom up) Approach; 4.2 Measurement Data for Uncertainty Calculation Using the ISO GUM Modelling Approach; 4.3 Equations for Uncertainty Calculation Using In-house Validation Data; 4.4 Data for Uncertainty Calculation Using In-house Validation Data; Exercise 1: Establishing Traceability in Analytical Chemistry; Exercise 2: Single Laboratory Validation of Measurement Procedures; Part I: General Issues; Part II: Parameters to Be Validated
• Publisher Details: Cham, Switzerland : Springer
• Publication Date: 2019
• Extent: 1 online resource (140 pages)
• Subjects: 543.072; Chemometrics; Electronic books
• Languages: English
• ISBNs: 9783030203474; 3030203476
• Access Rights: Legal Deposit; Only available on premises controlled by the deposit library and to one user at any one time; The Legal Deposit Libraries (Non-Print Works) Regulations (UK).
• Access Usage: Restricted: Printing from this resource is governed by The Legal Deposit Libraries (Non-Print Works) Regulations (UK) and UK copyright law currently in force.