Handbook of GC/MS : fundamentals and applications /: fundamentals and applications. (2015)

• Record Type: Book
• Further Information: Note: By Hans-Joachim Hübschmann.
• Authors: Hübschmann, Hans-Joachim
• Contents: Cover; Title Page; Copyright; Dedication; Contents; Foreword; Preface to the Third Edition; Chapter 1 Introduction; 1.1 The Historical Development of the GC-MS Technique; Chapter 2 Fundamentals; 2.1 Sample Preparation; 2.1.1 Solid Phase Extraction; 2.1.2 Solid Phase Microextraction; 2.1.3 Pressurized Liquid Extraction; 2.1.3.1 In-Cell Sample Preparation; 2.1.3.2 In-Cell Moisture Removal; 2.1.3.3 In-Cell Hydrocarbon Oxidation; 2.1.4 Online Liquid Chromatography Clean-Up; 2.1.5 Headspace Techniques; 2.1.5.1 Static Headspace Technique; 2.1.5.2 Dynamic Headspace Technique (Purge and Trap) 2.1.5.3 Coupling of Purge and Trap with GC-MS Systems2.1.5.4 Headspace versus Purge and Trap; 2.1.6 Adsorptive Enrichment and Thermal Desorption; 2.1.6.1 Sample Collection; 2.1.6.2 Calibration; 2.1.6.3 Desorption; 2.1.7 Pyrolysis; 2.1.7.1 Foil Pyrolysis; 2.1.7.2 Curie Point Pyrolysis; 2.1.7.3 Micro-furnace Pyrolysis; 2.1.8 Thermal Extraction (Outgassing); 2.1.9 QuEChERS Sample Preparation; 2.2 Gas Chromatography; 2.2.1 Sample Inlet Systems; 2.2.2 Carrier Gas Regulation; 2.2.2.1 Forward Pressure Regulation; 2.2.2.2 Back Pressure Regulation; 2.2.2.3 Carrier Gas Saving. 2.2.3 Injection Port Septa2.2.3.1 Septum Purge; 2.2.3.2 The MicroSeal Septum; 2.2.4 Injection Port Liner; 2.2.4.1 Split Injection; 2.2.4.2 Splitless Injection; 2.2.4.3 Liner Activity and Deactivation; 2.2.4.4 Liner Geometry; 2.2.5 Vaporizing Sample Injection Techniques; 2.2.5.1 Hot Needle Thermo Spray Injection Technique; 2.2.5.2 Cold Needle Liquid Band Injection Technique; 2.2.5.3 Filled Needle Injections; 2.2.5.4 Split Injection; 2.2.5.5 Splitless Injection (Total Sample Transfer); 2.2.5.6 Concurrent Solvent Recondensation; 2.2.5.7 Concurrent Backflush. 2.2.6 Temperature Programmable Injection Systems2.2.6.1 The PTV Cold Injection System; 2.2.6.2 The PTV Injection Procedures; 2.2.6.3 On-Column Injection; 2.2.6.4 PTV On-Column Injection; 2.2.6.5 Cryofocussing; 2.2.6.6 PTV Cryo-Enrichment; 2.2.7 Capillary Column Choice and Separation Optimization; 2.2.7.1 Sample Capacity; 2.2.7.2 Internal Diameter; 2.2.7.3 Film Thickness; 2.2.7.4 Column Length; 2.2.7.5 Setting the Carrier Gas Flow; 2.2.7.6 Properties of Column Phases; 2.2.7.7 Properties of Ionic Liquid Phases; 2.2.8 Chromatography Parameters; 2.2.8.1 The Chromatogram and Its Meaning. 2.2.8.2 Capacity Factor k'2.2.8.3 Chromatographic Resolution; 2.2.8.4 Factors Affecting the Resolution; 2.2.8.5 Maximum Sample Capacity; 2.2.8.6 Peak Symmetry; 2.2.8.7 Optimization of Carrier Gas Flow; 2.2.8.8 Effect of Oven Temperature Ramp Rate; 2.2.9 Fast Gas Chromatography Solutions; 2.2.9.1 Fast Chromatography; 2.2.9.2 Ultra-Fast Chromatography; 2.2.10 Multi-Dimensional Gas Chromatography; 2.2.10.1 Heart Cutting; 2.2.10.2 Comprehensive GC -- GC x GC; 2.2.10.3 Modulation; 2.2.10.4 Detection; 2.2.10.5 Data Handling; 2.2.10.6 Moving Capillary Stream Switching.
• Edition: Third edition
• Publisher Details: Weinheim : Wiley-VCH
• Publication Date: 2015
• Extent: 1 online resource
• Subjects: 543.85; Gas chromatography; Mass spectrometry; SCIENCE -- Chemistry -- Analytic; Gas chromatography; Mass spectrometry; Electronic books
• Languages: English
• ISBNs: 9783527674305; 3527674306; 9783527674336; 3527674330; 9783527674329; 3527674322; 9783527674312; 3527674314
• Related ISBNs: 9783527334742; 3527334742
• Notes: Note: Includes bibliographical references and index.; Note: Print version record.
• Access Rights: Legal Deposit; Only available on premises controlled by the deposit library and to one user at any one time; The Legal Deposit Libraries (Non-Print Works) Regulations (UK).
• Access Usage: Restricted: Printing from this resource is governed by The Legal Deposit Libraries (Non-Print Works) Regulations (UK) and UK copyright law currently in force.