Nanoscale AFM and TEM Observations of Elementary Dislocation Mechanisms. (2016)

• Record Type: Book
• Other Names: Vesel?y, Jozef
• Contents: Supervisor's Foreword; Abstract; Acknowledgments; Contents; Abbreviations; 1 Introduction; References; 2 Iron Rich Iron-Aluminides; 2.1 Structure; 2.1.1 Lattice Parameter; 2.1.2 Long-Range Order and Sublattice Occupancies; 2.1.3 Phase Transformations; 2.1.4 Short-Range Order and K-State; 2.2 Defects; 2.2.1 Point Defects: Vacancies and Anti-site Atoms; 2.2.2 Dislocations; 2.2.3 Anti-phase Domains and Boundaries; 2.3 Yield Stress Anomaly; References; 3 Experimental Methods; 3.1 Composition; 3.2 Bridgman Method; 3.3 Sample Cutting and Orientation; 3.4 Laue Back-Reflection X-Ray Diffraction. 3.5 Annealing3.6 Atomic Force Microscopy; 3.6.1 Contact and Tapping Mode; 3.6.2 Feedback Loop Tuning; 3.6.3 Sample Preparation; 3.6.4 In-Situ Deformation; 3.6.5 Step Fiting Method; 3.6.6 Drift and Image Alignment; 3.7 Transmission Electron Microscopy; 3.7.1 Diffraction Contrast; 3.7.2 Visibility of Dislocations; 3.7.3 Kikuchi Line Fitting; 3.7.4 Stereo Reconstruction; 3.7.5 Sample Preparation; References; 4 Observations of Dislocations and Other Results; 4.1 Deformation; 4.2 Order; 4.2.1 Selected Area Electron Diffraction; 4.2.2 Anti-phase Domains; 4.3 Carbide Particles; 4.4 Fe -- Al20. 4.4.1 TEM of Undeformed Material4.4.2 Wavy Slip; 4.4.3 Bowtie Structures; 4.5 Fe -- Al28; 4.5.1 TEM of Undeformed Material; 4.5.2 In-Situ AFM Observations; 4.5.3 AFM Observations of Samples Deformed at Different Temperatures; 4.5.4 TEM Observations of Samples Deformed at Diferent Temperatures; 4.6 Fe -- Al40; 4.6.1 Square Dislocation Loops in Undeformed Material; 4.6.2 In-Situ AFM Observations; 4.6.3 TEM Observations of Deformed Sample; 5 Discussion; 5.1 Deformation; 5.2 Order and Anti-phase Boundaries; 5.3 Carbides; 5.4 Fe -- Al20; 5.5 Fe -- Al28; 5.6 Fe -- Al40; References; 6 Summary; Reference. Appendix A Supplementary MaterialA. 1 Optical Images; A.2 In-situ Image Sequences; A.3 Interactive 3D Models; Curriculum Vitae.
• Publisher Details: Cham, SWITZERLAND : Springer
• Publication Date: 2016
• Extent: 1 online resource (112)
• Subjects: 530; Physics; Nanostructured materials; Nanostructured materials; Technology & Engineering -- Material Science; Science -- Solid State Physics; Science -- Mathematical Physics; Testing of materials; Materials / States of matter; Mathematical physics; Surfaces (Physics); Science -- Spectroscopy & Spectrum Analysis; Spectrum analysis, spectrochemistry, mass spectrometry; Electronic books
• Languages: English
• ISBNs: 3319483021; 9783319483023
• Related ISBNs: 3319483013
• Notes: Note: Print version record.
• Access Rights: Legal Deposit; Only available on premises controlled by the deposit library and to one user at any one time; The Legal Deposit Libraries (Non-Print Works) Regulations (UK).
• Access Usage: Restricted: Printing from this resource is governed by The Legal Deposit Libraries (Non-Print Works) Regulations (UK) and UK copyright law currently in force.