Liquid Chromatography for the Analyst. (1994)

• Record Type: Book
• Further Information: Note: Raymond P.W. Scott.
• Authors: Scott, Raymond P. W
• Contents: Cover; Half Title; Series Page; Title Page; Copyright Page; Preface; Acknowledgments; Table of Contents; 1. An Introduction to Chromatography; A Short History of LC; The Separation Process; The Different Forms of Chromatography; Chromatography Nomenclature; References; 2. Resolution, Retention and Selectivity; The Plate Theory; The Retention Volume of a Solute; Factors that Control the Distribution Coefficient of a Solute; Molecular Interactions; The Thermodynamic Explanation of Retention; Factors that Control the Availability of the Stationary Phase; Chromatographic Methods of Identification The Capacity Ratio of a SoluteThe Separation Ratio; Column Efficiency; References; 3. Liquid Chromatography Phase Systems; The Production of Silica Gel; Solute/Solvent Interactions on the Surface of Silica Gel; Mono-Layer Adsorption of Solvents on the Surface of Silica Gel; Solute Interactions with the Silica Gel Surface (Mobile Phase n-Heptane/Chloroform); Bi-Layer Adsorption of Solvents on the Surface of Silica Gel; Solute Interactions with the Silica Gel Surface (Mobile Phase n-Heptane/Ethyl Acetate); Silica Gel as an Exclusion Medium; Application Areas for Silica Gel as a Stationary Phase Silica Gel as a Stationary Phase in Elution ChromatographySilica Gel as a Stationary Phase in Exclusion Chromatography; Bonded Phases; The Different Classes of Bonded Phases; Reverse Phases; The Interaction of Reverse Phases with Solvents and Solutes; Paired Ion Reagents; The Use of Bonded Phases in Elution Chromatography; Aqueous Solvent Mixtures; The Use of Macro-Porous Polymers as Stationary Phases; Polymer Stationary Phases in Elution Chromatography; General Advice for the Unknown Sample; References; 4. The Liquid Chromatography Column; The Rate Theory; The Summation of Variances The Maximum Sample VolumeThe Van Deemter Equation; The Significance of the HETP Equation; The Reduced Chromatogram; Resolution; Calculating the Efficiency Required to Achieve a Specific Resolution; Peak Asymmetry; Column Selection; Column Diameter; Preparative Columns; Volume Overload; References; 5. The Liquid Chromatograph; The Basic Liquid Chromatograph; The Mobile Phase Supply System; The Gradient Programmer; The LC Pump; The Sample Valve; The Column and Column Oven; Detectors; Data Acquisition and Processing; References; 6. Liquid Chromatography Detectors; Detector Specifications Detector Linearity and Response Index (a)Linear Dynamic Range; Detector Noise Level; Measurement of Detector Noise; Detector Sensitivity or the Minimum Detectable Concentration; Pressure Sensitivity; Flow Sensitivity; Temperature Sensitivity; The UV Detector; The Fixed Wavelength Detector; The Multi-Wavelength Detector; The Electrical Conductivity Detector; The Fluorescence Detector; The Refractive Index Detector; The Tridet Multifunctional Detector; References; 7. Sample Preparation; Sample Preparation Techniques; Filtration Techniques; Centrifugation Techniques
• Publisher Details: Boca Raton, FL : CRC Press
• Publication Date: 1994
• Extent: 1 online resource
• Subjects: 543/.0894; Chromatographic analysis; Chromatographic analysis; Electronic books
• Languages: English
• ISBNs: 9781482277593
• Related ISBNs: 148227759X
• Access Rights: Legal Deposit; Only available on premises controlled by the deposit library and to one user at any one time; The Legal Deposit Libraries (Non-Print Works) Regulations (UK).
• Access Usage: Restricted: Printing from this resource is governed by The Legal Deposit Libraries (Non-Print Works) Regulations (UK) and UK copyright law currently in force.