Design, simulation and optimization of adsorptive and chromatographic separations : a hands-on approach /: a hands-on approach. ([2018])

• Record Type: Book
• Further Information: Note: Kevin R. Wood, Y.A. Liu and Yueying Yu.
• Authors: Wood, Kevin R; Liu, Y. A (Yih An); Yu, Yueying
• Contents: 1 SIMULATION OF ADSORPTION PROCESSES 4; 1.1 INTRODUCTION TO GAS-PHASE ADSORPTION TECHNOLOGIES 4; 1.2 CORE CONCEPTS IN GAS ADSORPTION 5; 1.2.1 THE ADSORPTION PROCESS 5; 1.2.2 HOW THE DRIVING FORCES ACHIEVE SEPARATION 6; 1.3 ISOTHERMS 7; 1.3.1 THE LANGMUIR ISOTHERM[8] (1918) 8; 1.3.2 THE LINEAR ISOTHERM 8; 1.3.3 THE BRUNAUER?EMMETT?TELLER (BET) ISOTHERM[9] (1938) 8; 1.3.4 THE FREUNDLICH ISOTHERM[10] (1906) 8; 1.3.5 THE SIPS (LANGMUIR-FREUNDLICH) ISOTHERM[11] (1948) 8; 1.3.6 THE TOTH ISOTHERM[12] (1971) 9; 1.3.7 SUMMARY 9; 1.4 THE PROPERTIES OF PACKED BEDS 9; 1.4.1 VOID FRACTIONS 10; 1.4.2 EXTERNAL VOIDS 11; 1.4.3 INTERNAL VOIDS 11; 1.4.4 DENSITIES 12; 1.4.5 RELATIONSHIPS 13; 1.4.6 GAS-PHASE BEHAVIOR 14; 1.5 PSA AND TSA IMPLEMENTATION DETAILS 15; 1.5.1 COMMON ADSORBENT CHARACTERISTICS 15; 1.5.2 COMMON PROCESS CONFIGURATIONS 16; 1.6 INTRODUCTION TO ASPEN ADSORPTION 18; 1.7 PSA WORKSHOP: ASPEN ADSORPTION MODELING FOR AIR SEPARATION 19; 1.7.1 ADDING COMPONENTS TO AN ASPEN ADSORPTION SIMULATION 21; 1.7.2 CREATING A FLOWSHEET IN ASPEN ADSORPTION 26; 1.7.3 SPECIFYING OPERATING CONDITIONS: TABLES AND FORMS 34; 1.7.4 SCHEDULING EVENTS WITH THE CYCLE ORGANIZER 43; 1.7.5 RUNNING AN ASPEN SIMULATION 56; 1.7.6 VIEWING AND EXPORTING SIMULATION RESULTS 56; 1.8 PSA WORKSHOP: HYDROGEN SEPARATION IN ASPEN ADSORPTION 60; 1.8.1 CREATING A FLOWSHEET IN ASPEN ADSORPTION 66; 1.8.2 RUN A BREAKTHOUGH SIMULATION 69; 1.8.3 CREATE THE PSA FLOWSHEET 81; 1.9 PSA WORKSHOP: MODELING HYDROGEN SEPARATION USING GCSS 92; 1.9.1 WORKING WITH MODEL LIBRARIES: ADVANCED FLOWSHEET OPTIONS 97; 1.9.2 INTRODUCTION TO SCRIPTING: SET REPEATED VALUES AND INITIALIZE BLOCKS 110; 1.9.3 INSPECTING BLOCKS: ADVANCED OPERATING CONDITIONS 112; 1.9.4 DEFINING THE CYCLE ORGANIZER 124; 1.9.5 VIEWING RESULTS 128; 1.10 CONCLUSIONS 130; 1.11 PRACTICE PROBLEMS 131; 1.11.1 INTRODUCING A GAS_INTERACTION UNIT INTO WORKSHOP 1 131; 1.11.2 NAPTHA UPGRADING USING ADSORPTION 132; 1.12 NOMENCLATURE 137; 1.13 FURTHER READING 139; 1.13.1 BOOKS 139; 1.13.2 JOURNAL ARTICLES SPECIFICALLY UTILIZING ASPEN ADSORPTION 139; 1.13.3 JOURNAL ARTICLES 141; 2 SIMULATION OF SMB CHROMATOGRAPHIC PROCESSES 144; 2.1 INTRODUCTION TO CHROMATOGRAPHY 144; 2.1.1 MATHEMATICAL DIFFERENCES FROM GAS ADSORPTION 144; 2.1.2 THERMODYNAMIC DIFFERENCES FROM GAS ADSORPTION 144; 2.2 INTRODUCTION TO SMB CHROMATOGRAPHY 145; 2.3 SMB IMPLEMENTATION DETAILS 146; 2.3.1 COMMON PROCESS CONFIGURATIONS 146; 2.3.2 M-VALUES 148; 2.3.3 SCALE-UP CONCERNS 149; 2.3.4 PRESSURE DROP LIMITATIONS 150; 2.3.5 INTRODUCTION TO OPERATIONAL MODES 151; 2.4 SMB WORKSHOP: SIMULATE A 4-ZONE SMB IN ASPEN CHROMATOGRAPHY FOR THE SEPARATION OF TRÖGERS?S BASE ENANTIOMERS 151; 2.4.1 CREATING A FLOWSHEET IN ASPEN CHROMATOGRAPHY 151; 2.4.2 ADDING COMPONENTS TO AN ASPEN CHROMATOGRAPHY SIMULATION 152; 2.4.3 THE CHROM_CCC_SEPARATOR2 BLOCK 153; 2.4.4 VIEWING RESULTS 177; 2.5 TANDEM SMB WORKSHOP: SIMULATE A SEPARATION WITH DUAL SMB COLUMNS 182; 2.6 PRACTICE PROBLEMS 192; 2.6.1 RUN WORKSHOP 2.4 AS A STEADY- STATE SIMULATION 192; 2.6.2 SIMULATION OF AN INDUSTRIAL-SCALE XYLENE SEPARATION USING LITERATURE DATA 193; 2.6.3 SIMULATE A 5-ZONE SMB SYSTEM FOR SEPARATING PHENYLALANINE, TRYPTOPHAN AND METHIONINE 196; 2.7 FURTHER READING 202; 2.7.1 BOOKS 202; 2.7.2 JOURNAL ARTICLES SPECIFICALLY UTILIZING ASPEN CHROMATOGRAPHY 202; 2.7.3 JOURNAL ARTICLES 205; 3 SHORTCUT DESIGN OF SMB SYSTEMS 209; 3.1 GENERAL CONCEPTS 209; 3.1.1 MASS BALANCES 211; 3.2 TRIANGLE THEORY 213; 3.2.1 NOTATION 213; 3.2.2 INTRODUCTION 214; 3.2.3 CONSTRAINTS ON THE SYSTEM 216; 3.3 TRIANGLE THEORY WORKSHOP: DESIGN OF A SYSTEM FOR THE SEPARATION OF AMINO ACIDS 217; 3.4 EXERCISE 1: CALCULATING TRANSITIONS IN A FIXED BED USING MATHEMATICA 228; 3.4.1 DIFFERENTIAL EQUATIONS ? ANALYSIS 228; 3.4.2 CONSTRUCTING THE SOLUTION FROM EIGENVECTORS AND EIGENVALUES 231; 3.4.3 USE THE STEADY- STATE INFORMATION TO CONSTRAIN OPERATING CONDITIONS 232; 3.4.4 EXERCISE 2: CONSTRUCTING THE CONSTRAINTS ON THE TMB SYSTEM IN MATHEMATICA 245; 3.5 STANDING WAVE DESIGN 249; 3.5.1 STANDING WAVE DESIGN IN A NONLINEAR IDEAL SYSTEM 250; 3.5.
• Publisher Details: Weinheim, Germany : Wiley-VCH
• Publication Date: 2018
• Extent: 1 online resource, illustrations
• Subjects: 541/.33; Adsorption -- Simulation methods; Chromatographic analysis -- Simulation methods; Separation (Technology); Chemistry, Analytic; SCIENCE / Chemistry / Physical & Theoretical; Electronic books
• Languages: English
• ISBNs: 9783527814992; 9783527815012; 3527815015
• Related ISBNs: 352781499X; 9783527344697
• Notes: Note: Includes bibliographical references and index.; Note: Online resource; title from PDF title page (EBSCO, viewed March 08, 2018).
• Access Rights: Legal Deposit; Only available on premises controlled by the deposit library and to one user at any one time; The Legal Deposit Libraries (Non-Print Works) Regulations (UK).
• Access Usage: Restricted: Printing from this resource is governed by The Legal Deposit Libraries (Non-Print Works) Regulations (UK) and UK copyright law currently in force.