Laboratory experiments using microwave heating. (2013)

• Record Type: Book
• Further Information: Note: Authors, Nicholas E. Leadbeater, Cynthia B. McGowan.
• Authors: Leadbeater, Nicholas E; McGowan, Cynthia B
• Contents: Introduction: Using microwave heating in chemistry: the basics -- Experiment 1: Diels-Alder cycloaddition reaction -- Experiment 2: Second-order elimination reaction: preparation of heptene from 2-bromoheptane -- Experiment 3: An addition-elimination sequence preparation of a bromoalkene -- Experiment 4: Fischer esterification: preparation of ethyl-4-aminobenzoate (benzocaine) -- Experiment 5: Transesterification reaction: preparation of biodiesel -- Experiment 6: Knoevenagel condensation reaction: preparation of 3-acetylcoumarin -- Experiment 7: The Perkin reaction: condensation of an aromatic aldehyde with rhodanine -- Experiment 8: Williamson ether synthesis: preparation of allyl phenyl ether -- Experiment 9: Claisen rearrangement: preparation of 2-allyl phenol from allyl phenyl ether -- Experiment 10: Hydration of an alkyne: preparation of acetophenone from phenylacetylene -- Experiment 11: Oxidation of secondary alcohol: preparation of a ketone -- Experiment 12: Suzuki coupling reaction:preparation of a biaryl -- Experiment 13: Heck reaction: preparation of substituted cinnamic acids -- Experiment 14: Preparation of an aryl nitrile: application of a copper-catalyzed cyanation reaction -- Experiment 15: Alkene metathesis: preparation of a substituted cyclopentene -- Experiment 16: Click reaction: preparation of a triazole -- Experiment 17: Coordination chemistry: preparation of cisplatin -- Experiment 18: Preparation of a palladium complex: bis(triphenylphosphine)palladium(II) dichloride -- Experiment 19: Coordination of an aromatic ring to a metal: preparation of an arene chromium tricarbonyl complex -- Experiment 20: Determination of an empirical formula: zinc bromide -- Experiment 21: Microwave-assisted extraction: identification of the major flavor components of citrus oil -- Experiment 22: Microwave-assisted digestion of dietary supplements: metal analysis by atomic absorption spectroscopy.
• Publisher Details: Boca Raton : Taylor & Francis
• Publication Date: 2013
• Extent: 1 online resource (234 pages)
• Subjects: 660.28; Chemistry -- Experiments; Chemistry -- Laboratory manuals; Microwaves -- Industrial applications; Microwave heating; Chemistry; Chemistry -- Experiments; Microwave heating; Microwaves -- Industrial applications; SCIENCE -- Chemistry -- General; SCIENCE -- Chemistry -- Organic; Laboratory manuals; Electronic books; Electronic books
• Languages: English
• ISBNs: 9781439856109; 1439856109; 9781498722513; 1498722512; 1299704077; 9781299704077
• Related ISBNs: 9781439856093; 1439856095
• Notes: Note: Description based on print version record.
• Access Rights: Legal Deposit; Only available on premises controlled by the deposit library and to one user at any one time; The Legal Deposit Libraries (Non-Print Works) Regulations (UK).
• Access Usage: Restricted: Printing from this resource is governed by The Legal Deposit Libraries (Non-Print Works) Regulations (UK) and UK copyright law currently in force.