Spectroscopic methods for nanomaterials characterization. ([2017])

• Record Type: Book
• Further Information: Note: Edited by Sabu Thomas, Raju Thomas, Ajesh K. Zachariah, Raghvendra Kumar Mishra.
• Editors: Thomas, Sabu; Thomas, Raju; Zachariah, Ajesh K, 1983-; Mishra, Raghvendra Kumar
• Contents: Front Cover; Spectroscopic Methods for Nanomaterials Characterization; Spectroscopic Methods for Nanomaterials Characterization; Copyright; Contents; List of Contributors; Editor Biographies; 1 -- Atomic Force Microscopy as a Nanoanalytical Tool; 1.1 INTRODUCTION; 1.2 SPECIMEN PREPARATION; 1.2.1 Thin Films; 1.2.2 Physical and Chemical Etching, Ion Etching; 1.2.3 Ultramicrotomy; 1.3 TYPICAL EXAMPLES OF NANOMATERIALS CHARACTERIZATION BY ATOMIC FORCE MICROSCOPY; 1.3.1 Nanoparticles Imaging and Manipulation; 1.3.2 Biobased Nanomaterials and Nanoencapsulation 1.3.3 Comparison With Electron Microscopy1.4 CONCLUDING REMARKS; ACKNOWLEDGMENTS; REFERENCES; 2 -- Electrochemical Characterization; 2.1 INTRODUCTION; 2.2 ELECTROCHEMICAL CELL; 2.3 ELECTROCHEMICAL CHARACTERIZATION; 2.3.1 Voltammetric Techniques; 2.3.1.1 Polarography; 2.3.1.2 Differential Pulse Voltammetry; 2.3.1.3 Hydrodynamic Voltammetry; 2.3.1.4 Stripping Voltammetry; 2.3.1.5 Cyclic Voltammetry; 2.3.1.6 Square-Wave Voltammetry; 2.3.1.7 Staircase Voltammetry; 2.3.2 Electrochemical Impedance Spectroscopy; 2.3.3 Galvanostatic Charge-Discharge; 2.3.4 Chronopotentiometry; 2.3.5 Chronoamperometry 2.3.6 Coulometry2.3.7 Chronocoulometry; 2.3.8 Scanning Electrochemical Microscope; 2.4 APPLICATIONS; 2.4.1 Supercapacitors and Batteries; 2.4.2 Sensor Studies; 2.4.3 Coatings; 2.5 SUMMARY; REFERENCES; 3 -- Ultraviolet Spectroscopy: A Facile Approach for the Characterization of Nanomaterials; 3.1 INTRODUCTION; 3.2 SPECTROCHEMICAL METHODS; 3.2.1 Absorption Laws; 3.2.2 Ultraviolet Spectroscopy; 3.3 NANOMATERIALS; 3.3.1 Classification of Nanoparticles; 3.3.1.1 Zero-Dimensional Nanomaterials; 3.3.1.2 One-Dimensional Nanomaterials; 3.3.1.3 Two-Dimensional Nanoparticles 3.3.1.4 Three-Dimensional Nanoparticles3.4 CHARACTERIZATION OF NANOPARTICLES; 3.5 ADVANTAGES OF UV SPECTROSCOPY; 3.6 CHARACTERIZATION OF NANOPARTICLES USING UV SPECTROSCOPY; 3.7 CONCLUSIONS; REFERENCES; 4 -- Fourier Transform Infrared Spectroscopy; 4.1 INTRODUCTION; 4.2 WORKING PRINCIPLE; 4.3 SAMPLE ANALYSIS PROCESS; 4.3.1 Instrumentation; 4.3.2 Sample Preparation; 4.3.3 Working of a Fourier Transform Infrared Spectrometer; 4.3.4 Sample Preparation Techniques; 4.3.4.1 Gas Samples; 4.3.4.2 Liquid Samples; 4.3.4.3 Solid Samples; 4.3.5 Alkali Halide Disks; 4.3.6 Mulls 4.4 ANALYTICAL INFORMATION FOR FOURIER TRANSFORM INFRARED [2]4.4.1 Qualitative Analysis; 4.4.1.1 Structural Elucidation; 4.4.1.2 Compound Identification; 4.4.2 Quantitative Analysis; 4.5 INTERPRETATION AND ANALYSIS OF THE INFRARED SPECTRUM; 4.6 INTERPRETING SOME FUNCTIONAL GROUPS; 4.6.1 Hydrocarbons; 4.6.2 Aromatic Compounds; 4.6.3 Nitriles and Alkynes; 4.6.4 Alcohols and Amines; 4.6.5 Ethers; 4.6.6 Carbonyl Compounds; 4.6.7 Aldehydes; 4.6.8 Carboxylic Acids; 4.7 SIGNIFICANCE AND DRAWBACK OF FOURIER TRANSFORM INFRARED; 4.7.1 Significance; 4.7.1.1 Speed; 4.7.1.2 Sensitivity; 4.7.1.3 Simplicity
• Publisher Details: Amsterdam Kidlington, Oxford Cambridge, MA : Elsevier Ltd
• Publication Date: 2017
• Copyright Date: 2017
• Extent: 1 online resource (xx, 424 pages)
• Subjects: 620.1/157; Nanostructured materials -- Spectra; TECHNOLOGY & ENGINEERING / Engineering (General); TECHNOLOGY & ENGINEERING / Reference; Electronic books
• Languages: English
• ISBNs: 9780323461467; 0323461468
• Related ISBNs: 9780323461405; 0323461409
• Notes: Note: Includes bibliographical references and index.; Note: Description based on online resource; title from digital title page (viewed on June 15, 2017).
• Access Rights: Legal Deposit; Only available on premises controlled by the deposit library and to one user at any one time; The Legal Deposit Libraries (Non-Print Works) Regulations (UK).
• Access Usage: Restricted: Printing from this resource is governed by The Legal Deposit Libraries (Non-Print Works) Regulations (UK) and UK copyright law currently in force.