Undergraduate instrumental analysis. (2014)

• Record Type: Book
• Authors: Frame, Eileen M. Skelly, 1953-; II, Frame, George M; Robinson, James W, 1923-
• Contents: Concepts of Instrumental Analytical Chemistry ; Introduction: What is Analytical Chemistry?; Analytical Approach; Basic Statistics and Data Handling; Sample Preparation; Performing the Measurement; Assessing the Data; Problems; Bibliography; ; Introduction to Spectroscopy; Interaction Between Electromagnetic Radiation and Matter; Atoms and Atomic Spectroscopy; Molecules and Molecular Spectroscopy; Absorption Laws; Methods of Calibration; Optical Systems Used in Spectroscopy; Spectroscopic Technique and Instrument Nomenclature; Suggested experiments; Problems; Bibliography; ; Magnetic Resonance Spectroscopy; Nuclear Magnetic Resonance Spectroscopy Introduction; The FTNMR Experiment; Chemical Shifts; Spin–Spin Coupling; Instrumentation; Analytical Applications of NMR; Hyphenated NMR Techniques; NMR Imaging and MRI; Time Domain NMR; Low-Field, Portable, and Miniature NMR Instruments; Limitations of NMR; Electron Spin Resonance Spectroscopy; Suggested Experiments; Problems; Spectral Databases; Bibliography; ; Infrared, Near-Infrared, and Raman Spectroscopy; Absorption of IR Radiation by Molecules; IR Instrumentation; Sampling Techniques; FTIR Microscopy; Nondispersive IR Systems; Analytical Applications of IR Spectroscopy; NIR Spectroscopy; Raman Spectroscopy; Chemical Imaging Using NIR, IR, and Raman Spectroscopy; Suggested Experiments; Problems; Bibliography; Spectral Databases; ; Visible and Ultraviolet Molecular Spectroscopy; Introduction; Instrumentation; UV Absorption Spectra of Molecules; UV Spectra and the Structure of Organic Molecules; Analytical Applications; Accuracy and Precision in UV/Vis Absorption Spectrometry; Nephelometry and Turbidimetry; Molecular Emission Spectrometry; Instrumentation for Luminescence Measurements; Analytical Applications of Luminescence; Suggested Experiments; Problems; Bibliography; ; Atomic Absorption Spectrometry ; Absorption of Radiant Energy by Atoms; Instrumentation; Atomization Process; Interferences in AAS; Analytical Applications of AAS; Suggested Experiments; Problems; Appendices; Bibliography; ; Atomic Emission Spectroscopy ; Flame Atomic Emission Spectroscopy; Atomic OES; Plasma Emission Spectroscopy; GD Emission Spectrometry; AFS; Commercial Atomic Emission Systems; Laser-Induced Breakdown Spectroscopy; Atomic Emission Literature and Resources; Comparison of Atomic Spectroscopic and ICP-MS Techniques; Suggested experiments; Problems; Appendices; Bibliography; ; X-Ray Spectroscopy (Contributing authors: Alexander Seyfarth and Eileen Skelly Frame); Origin of X-Ray Spectra; X-Ray Fluorescence; X-Ray Absorption; X-Ray Diffraction; X-Ray Emission; Commercial X-Ray Instrument Manufacturers; Suggested Experiments; Problems; Appendices; Bibliography; ; Mass Spectrometry I: Principles and Instrumentation; Principles of MS; Instrumentation; Ion Mobility Spectrometry; Problems; Bibliography; ; Mass Spectrometry II: Spectral Interpretation and Applications; Interpretation of Mass Spectra: Structural Determination of Simple Molecules; Mass Spectral Interpretation: Some Examples; Applications of Molecular MS; Atomic MS; Problems; Appendix; Bibliography; ; Principles of Chromatography; Introduction to Chromatography; What is the Chromatographic Process?; Chromatography in More than One Dimension; Visualization of the Chromatographic Process at the Molecular Level: Analogy to "People on a Moving Belt Slideway"; Digression on the Central Role of Silicon–Oxygen Compounds in Chromatography; Basic Equations Describing Chromatographic Separations; How Do Column Variables Affect Efficiency (Plate Height)?; Practical Optimization of Chromatographic Separations; Extra-Column Band Broadening Effects; Qualitative Chromatography: Analyte Identification; Quantitative Measurements in Chromatography; Examples of Chromatographic Calculations ; Problems; Bibliography; ; Gas Chromatography; Historical Development of GC: The First Chromatographic Instrumentation; Advances in GC Leading to Present-Day Instrumentation; GC Instrument Component Design (Injectors); GC Instrument Component Design (The Column); GC Instrument Operation (Column Dimensions and Elution Values); GC Instrument Operation (Column Temperature and Elution Values); GC Instrument Component Design (Detectors); Hyphenated GC Techniques (GC-MS, GC-IR, GC-GC, or D-GC); Retention Indices (A Generalization of Relative Rt Information); Scope of GC Analyses; Problems; Appendix 12.1; Bibliography; ; Chromatography with Liquid Mobile Phases ; High-Performance Liquid Chromatography; Chromatography of Ions Dissolved in Liquids; Affinity Chromatography; Size-Exclusion Chromatography; Supercritical Fluid Chromatography; Electrophoresis; Planar Chromatography and Planar Electrophoresis; Problems and Exercises; Appendix 13.A; Bibliography; ; Surface Analysis; Introduction; Electron Spectroscopy Techniques; Ion Scattering Spectroscopy; Secondary Ion Mass Spectrometry; Electron Microprobe (Electron Probe Microanalysis); Problems; Bibliography; ; Electroanalytical Chemistry ; Fundamentals of Electrochemistry; Electrochemical Cells; Electroanalytical Methods; Liquid Chromatography Detectors; Spectroelectrochemistry; Quartz Crystal Microbalance; Suggested Experiments; Problems; Appendix 15.A; Bibliography; ; Thermal Analysis; Thermogravimetry; Differential Thermal Analysis; Differential Scanning Calorimetry ; Hyphenated Techniques&l
• Edition: 7th edition
• Publisher Details: Boca Raton : CRC Press
• Publication Date: 2014
• Extent: 1 online resource, illustrations (black and white)
• Subjects: 543.19; Instrumental analysis
• Languages: English
• ISBNs: 9781482233742
• Related ISBNs: 9781420061369
• Notes: Note: Description based on CIP data; resource not viewed.
• Access Rights: Legal Deposit; Only available on premises controlled by the deposit library and to one user at any one time; The Legal Deposit Libraries (Non-Print Works) Regulations (UK).
• Access Usage: Restricted: Printing from this resource is governed by The Legal Deposit Libraries (Non-Print Works) Regulations (UK) and UK copyright law currently in force.